Carbamic acid, [1-[(1S,2R,4R)-4-[[(1,1-dimethylethoxy)carbonyl]amino]-2-(hydroxymeth yl)cyclohexyl]-2-oxo-3-pyrrolidinyl]-, phenylmethyl ester

Base Information

Chemical Name:Carbamic acid, [1-[(1S,2R,4R)-4-[[(1,1-dimethylethoxy)carbonyl]amino]-2-(hydroxymeth yl)cyclohexyl]-2-oxo-3-pyrrolidinyl]-, phenylmethyl ester
CAS No.:746671-23-8
Molecular Formula:C24H35N3O6
Molecular Weight:461.558
Hs Code.:

Carbamic acid,
[1-[(1S,2R,4R)-4-[[(1,1-dimethylethoxy)carbonyl]amino]-2-(hydroxymeth
yl)cyclohexyl]-2-oxo-3-pyrrolidinyl]-, phenylmethyl ester

Synonyms:

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Chemical Property of Carbamic acid, [1-[(1S,2R,4R)-4-[[(1,1-dimethylethoxy)carbonyl]amino]-2-(hydroxymeth yl)cyclohexyl]-2-oxo-3-pyrrolidinyl]-, phenylmethyl ester

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Technology Process of Carbamic acid, [1-[(1S,2R,4R)-4-[[(1,1-dimethylethoxy)carbonyl]amino]-2-(hydroxymeth yl)cyclohexyl]-2-oxo-3-pyrrolidinyl]-, phenylmethyl ester

There total 1 articles about Carbamic acid, [1-[(1S,2R,4R)-4-[[(1,1-dimethylethoxy)carbonyl]amino]-2-(hydroxymeth yl)cyclohexyl]-2-oxo-3-pyrrolidinyl]-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 746671-17-0
tert-butyl (1R,2S,5R)-2-((S)-3-(((benzyloxy)carbonyl)amino)-2-oxopyrrolidin-1-yl)-7-oxo-6-azabicyclo[3.2.1]octane-6-carboxylate

: 746671-23-8
tert-butyl (1R,3R,4S)-4-((S)-3-benzyloxycarbonylamino-2-oxopyrrolidin-1-yl)-3-(hydroxymethyl)cyclohexylcarbamate

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; water; at 20 ℃; for 5h;

Reference yield:

: 746671-23-8
tert-butyl (1R,3R,4S)-4-((S)-3-benzyloxycarbonylamino-2-oxopyrrolidin-1-yl)-3-(hydroxymethyl)cyclohexylcarbamate

: 848002-44-8
tert-butyl (1R,4S)-4-((S)-3-benzyloxycarbonylamino-2-oxopyrrolidin-1-yl)-3-formylcyclohexylcarbamate

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.583333h;

tert-butyl (1R,3R,4S)-4-((S)-3-benzyloxycarbonylamino-2-oxopyrrolidin-1-yl)-3-(hydroxymethyl)cyclohexylcarbamate; In dichloromethane; at -78 ℃; for 1.08333h;

With triethylamine; In dichloromethane; at 0 ℃; for 2h;