1,2-Cyclohexanedicarboxylic acid, monomethyl ester

Base Information

• Chemical Name: 1,2-Cyclohexanedicarboxylic acid, monomethyl ester
• CAS No.: 7719-08-6
• Molecular Formula: C9H14O4
• Molecular Weight: 186.208

Synonyms:cyclohexane-1,2-dicarboxylic acid monomethyl ester;methyl hydrogen 1,2-cyclohexanedicarboxylate;trans-1,2-cyclohexanedicarboxylic acid, monomethyl ester;2-(methoxycarbonyl)cyclohexane-1-carboxylic acid;(trans)-1,2-cyclohexanedicarboxylic acid,mono(methyl)ester;Cyclohexan-1,2-dicarbonsaeure-monomethylester;

Chemical Property of 1,2-Cyclohexanedicarboxylic acid, monomethyl ester

Chemical Property:

• PSA: 63.60000
• LogP: 1.05040

Purity/Quality:

99%, ^*data from raw suppliers

2-(Methoxycarbonyl)cyclohexanecarboxylicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,2-Cyclohexanedicarboxylic acid, monomethyl ester

There total 25 articles about 1,2-Cyclohexanedicarboxylic acid, monomethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methanol (67-56-1) + 1,2-cis-cyclohexanedicarboxylic anhydride (13149-00-3) → cyclohexane-1,2-dicarboxylic acid monomethyl ester (2484-60-8,2778-62-3,7719-08-6,52782-07-7,88335-91-5,88335-92-6,96894-64-3,111955-05-6)

Guidance literature:

at 100 ℃; for 1h;

DOI:10.2174/1570178614666171130161203

Reference yield: 94.0%

cyclohexane-1,2-dicarboxylic acid monomethyl ester (2484-60-8,2778-62-3,7719-08-6,52782-07-7,88335-91-5,88335-92-6,96894-64-3,111955-05-6) → (1S*,2S*)-2-(methoxycarbonyl)cyclohexane-1-carboxylic acid (2484-60-8,2778-62-3,7719-08-6,52782-07-7,88335-91-5,88335-92-6,96894-64-3,111955-05-6)

Guidance literature:

With sodium methylate; In methanol; for 5h; Inert atmosphere; Reflux;

DOI:10.2174/1570178614666171130161203

Reference yield: 90.0%

Monomethyl phthalate (4376-18-5) → trans-1,2-cyclohexanedicarboxylic acid,monomethyl ester (7719-08-6)

Guidance literature:

With palladium on activated charcoal; hydrogen; In ethanol; at 20 ℃; for 5h; under 735.576 Torr;

upstream raw materials:

dimethyl 1,2-cyclohexanedicarboxylate

methyl iodide

C₁₀H₁₄O₄^(2-)*2Li⁽¹⁺⁾

methanol

Downstream raw materials:

(1S,2R)-2-(1,3-Dioxo-1,3-dihydro-isoindol-2-ylmethyl)-cyclohexanecarboxylic acid

methyl 2-(3-phenylpropylcarbamoyl)-cyclohexanecarboxylate

methyl cyclohex-1-ene-1-carboxylate

methyl cyclohex-2-en-1-carboxylate

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