Naphthalenecarboxylic acid, 1-bromo-, ethyl ester

Base Information

Chemical Name:Naphthalenecarboxylic acid, 1-bromo-, ethyl ester
CAS No.:773134-84-2
Molecular Formula:C13H11BrO2
Molecular Weight:279.12900
Hs Code.:
Mol file:773134-84-2.mol

Synonyms:1-bromo-[2]naphthoic acid ethyl ester;ethyl 2-(1-bromonaphthalene)carboxylate;ethyl bromonaphthalene-2-carboxylate;1-bromo-naphthalene-2-carboxylic acid ethyl ester;1-Brom-[2]naphthoesaeure-aethylester;

Suppliers and Price of Naphthalenecarboxylic acid, 1-bromo-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 10 raw suppliers

Chemical Property of Naphthalenecarboxylic acid, 1-bromo-, ethyl ester

Chemical Property:

Melting Point:36 - 37 °C (petroleum ether)
Boiling Point:363.4±15.0 °C(Predicted)
PSA：26.30000
Density:1.437±0.06 g/cm3(Predicted)
LogP:3.77900
Storage Temp.:2-8°C

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Naphthalenecarboxylic acid, 1-bromo-, ethyl ester

There total 5 articles about Naphthalenecarboxylic acid, 1-bromo-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.99%

: 64-17-5
ethanol

: 20717-79-7
1-bromo-2-naphthoic acid

: 773134-84-2
1-bromonaphthalene-2-carboxylic acid ethyl ester

Guidance literature:: With hydrogenchloride;
DOI:10.5012/bkcs.2011.32.5.1475

Reference yield: 95.0%

: 20717-79-7
1-bromo-2-naphthoic acid

: 75-03-6
ethyl iodide

: 773134-84-2
1-bromonaphthalene-2-carboxylic acid ethyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 2586-62-1
1-bromo-2-methylnaphtalene

: 773134-84-2
1-bromonaphthalene-2-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane

2: potassium acetate / acetic acid

3: 2-methyl-but-2-ene; tert-butyl alcohol

4: hydrogenchloride

With hydrogenchloride; N-Bromosuccinimide; 2-methyl-but-2-ene; 2,2'-azobis(isobutyronitrile); potassium acetate; tert-butyl alcohol; In tetrachloromethane; acetic acid;
DOI:10.5012/bkcs.2011.32.5.1475