Carbamic acid, [[(5S)-3-[3,5-difluoro-4-[(1a,5a,6a)-3-thiabicyclo[3.1.0]hex-6-yl]phenyl]- 2-oxo-5-oxazolidinyl]methyl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, [[(5S)-3-[3,5-difluoro-4-[(1a,5a,6a)-3-thiabicyclo[3.1.0]hex-6-yl]phenyl]- 2-oxo-5-oxazolidinyl]methyl]-, 1,1-dimethylethyl ester
CAS No.:777089-90-4
Molecular Formula:C₂₀H₂₄F₂N₂O₄S
Molecular Weight:426.484
Hs Code.:

Carbamic acid,
[[(5S)-3-[3,5-difluoro-4-[(1a,5a,6a)-3-thiabicyclo[3.1.0]hex-6-yl]phenyl]-
2-oxo-5-oxazolidinyl]methyl]-, 1,1-dimethylethyl ester

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamic acid, [[(5S)-3-[3,5-difluoro-4-[(1a,5a,6a)-3-thiabicyclo[3.1.0]hex-6-yl]phenyl]- 2-oxo-5-oxazolidinyl]methyl]-, 1,1-dimethylethyl ester

Chemical Property:

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Hazard Codes:

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Technology Process of Carbamic acid, [[(5S)-3-[3,5-difluoro-4-[(1a,5a,6a)-3-thiabicyclo[3.1.0]hex-6-yl]phenyl]- 2-oxo-5-oxazolidinyl]methyl]-, 1,1-dimethylethyl ester

There total 1 articles about Carbamic acid, [[(5S)-3-[3,5-difluoro-4-[(1a,5a,6a)-3-thiabicyclo[3.1.0]hex-6-yl]phenyl]- 2-oxo-5-oxazolidinyl]methyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 777089-89-1
((1S,5R,6S)-3,5-Difluoro-4-3-thia-bicyclo[3.1.0]hex-6-yl-phenyl)-carbamic acid benzyl ester

: 415684-05-8
tert-butyl (2S)-3-chloro-2-hydroxypropylcarbamate

: 777089-90-4
[(S)-3-((1S,5R,6S)-3,5-Difluoro-4-3-thia-bicyclo[3.1.0]hex-6-yl-phenyl)-2-oxo-oxazolidin-5-ylmethyl]-carbamic acid tert-butyl ester

Guidance literature:: With lithium tert-butoxide; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2005.11.093

Reference yield:

: 777089-90-4
[(S)-3-((1S,5R,6S)-3,5-Difluoro-4-3-thia-bicyclo[3.1.0]hex-6-yl-phenyl)-2-oxo-oxazolidin-5-ylmethyl]-carbamic acid tert-butyl ester

: 777090-08-1
(S)-5-Aminomethyl-3-((1S,5R,6S)-3,5-difluoro-4-3-thia-bicyclo[3.1.0]hex-6-yl-phenyl)-oxazolidin-2-one

Guidance literature:: With trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.bmcl.2005.11.093

Reference yield:

: 777089-90-4
[(S)-3-((1S,5R,6S)-3,5-Difluoro-4-3-thia-bicyclo[3.1.0]hex-6-yl-phenyl)-2-oxo-oxazolidin-5-ylmethyl]-carbamic acid tert-butyl ester

: 777089-91-5
N-[(S)-3-((1S,5R,6S)-3,5-Difluoro-4-3-thia-bicyclo[3.1.0]hex-6-yl-phenyl)-2-oxo-oxazolidin-5-ylmethyl]-propionamide

Guidance literature:: Multi-step reaction with 2 steps

1: TFA / CH₂Cl₂

2: dimethylformamide

With trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2005.11.093