Silane, (bromomethyl)dimethyl(phenylmethyl)-

Base Information

Chemical Name:Silane, (bromomethyl)dimethyl(phenylmethyl)-
CAS No.:77861-50-8
Molecular Formula:C₁₀H₁₅BrSi
Molecular Weight:243.219
Hs Code.:

Synonyms:

Suppliers and Price of Silane, (bromomethyl)dimethyl(phenylmethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Silane, (bromomethyl)dimethyl(phenylmethyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Silane, (bromomethyl)dimethyl(phenylmethyl)-

There total 2 articles about Silane, (bromomethyl)dimethyl(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 16532-02-8
bromomethyldimethylsilyl chloride

: 1589-82-8
phenylmagnesium bromide

: 77861-50-8
benzyl(bromomethyl)dimethylsilane

Guidance literature:: In diethyl ether;
DOI:10.1016/j.jorganchem.2011.05.011

Reference yield: 86.0%

: 16532-02-8
bromomethyldimethylsilyl chloride

: 6921-34-2
benzylmagnesium chloride

: 77861-50-8
benzyl(bromomethyl)dimethylsilane

Guidance literature:: In diethyl ether; for 8h; Heating;
DOI:10.1016/S0022-328X(00)88969-X

Reference yield:

: 7646-78-8
tin(IV) chloride

: 7439-95-4
magnesium

: 77861-50-8
benzyl(bromomethyl)dimethylsilane

: 215363-09-0
tris[(benzyldimethylsilyl)methylene]tin chloride

: 1322150-93-5
bis[(dimethyl(benzyl)silyl)methyl]tin dichloride

Guidance literature:: In diethyl ether; benzene; Ar, Et2O soln. of ligand (0.0217 mmol) added to Mg turnings in Et2O, mixt. stirred for 15 h at room temp., benzene soln. of SnCl4 (0.088 mmol) added dropwise at 0°C, mixt. stirred at room temp. for 1 h, refluxed for 4 h; cooled to room temp., treated with satd. aq. NH4Cl, org. layer septd., aq. layer washed (Et2O), combined org. soln. dried (MgSO4), evapd., chromd. (SiO2, 30% ethylacetate in n-hexane), elem. anal.;
DOI:10.1016/j.jorganchem.2011.05.011