Tetragermetane, octaethyl-

Base Information

Chemical Name:Tetragermetane, octaethyl-
CAS No.:79411-55-5
Molecular Formula:C16H40Ge4
Molecular Weight:522.854
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Tetragermetane, octaethyl-

Chemical Property:

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Technology Process of Tetragermetane, octaethyl-

There total 2 articles about Tetragermetane, octaethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 151920-23-9
1,1,2,2-tetraphenyl 1,2-digermyldilithium

: 151920-34-2
((C₂H₅)2(CH₃O)Ge)2

: 79411-55-5
((CH₃CH₂)2Ge)4

: 151920-33-1
(Ge(C₆H₅)2)2(Ge(C₂H₅)2)2

Guidance literature:: With hydrogenchloride; water; In tetrahydrofuran; byproducts: LiOCH3; under Ar or N2, addn. of the org. compd. in THF to a soln. of the digermyl compd. at -40°C, heated to ambient temp. and stirred for 8 h at 20°C, hydrolyzed (5% HCl); extn., drying, concg. in vac., crystn. (ether/pentane, at -30°C);
DOI:10.1016/S0020-1693(00)92307-7

Reference yield: 11.0%

: 993-84-0
pentaethyldigermane

: 110-05-4
di-tert-butyl peroxide

: 52119-02-5
tetraethyldigermane

: 79411-55-5
((CH₃CH₂)2Ge)4

: 925-90-6
ethylmagnesium bromide

: 13937-05-8
octaethyltrigermane

Guidance literature:: In benzene; Irradiation (UV/VIS); digermane soln. irradiating in the presence of an excess of t-Bu2O2; product content detd. by high-pressure chromy.;
DOI:10.1016/0022-328X(84)85145-1

Reference yield:

: 79411-55-5
((CH₃CH₂)2Ge)4

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: 67548-87-2
1,1,3,3,5,5-hexaethylcyclotrigermoxane

: 91123-36-3
((CH₃CH₂)2Ge)6

: 79411-56-6
((CH₃CH₂)2Ge)5

: 5764-67-0
1,1-Diethyl-3,4-dimethyl-1-germacyclopent-3-en

Guidance literature:: In benzene; Irradiation (UV/VIS); irradiating for 6 h in the presence of an excess of diene; detd. by high-pressure chromy.;
DOI:10.1016/0022-328X(84)85145-1