4-chloro-2-(morpholin-4-ylmethyl)phenol

Base Information

• Chemical Name: 4-chloro-2-(morpholin-4-ylmethyl)phenol
• CAS No.: 77802-87-0
• Molecular Formula: C11H14 Cl N O2
• Molecular Weight: 227.691
• Hs Code.: 2934999090
• Mol file: 77802-87-0.mol

Synonyms:4-Chloro-2-(morpholinomethyl)phenol;NSC 14846

Chemical Property of 4-chloro-2-(morpholin-4-ylmethyl)phenol

Chemical Property:

• Vapor Pressure: 5.47E-05mmHg at 25°C
• Boiling Point: 337.1°C at 760 mmHg
• Flash Point: 157.7°C
• PSA: 32.70000
• Density: 1.284g/cm³
• LogP: 1.81570

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-chloro-2-(morpholin-4-ylmethyl)phenol

There total 7 articles about 4-chloro-2-(morpholin-4-ylmethyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

potassium (morpholin-4-yl)methyltrifluoroborate + 4-chloro-phenol (106-48-9,82344-39-6) → 4-chloro-2-(N-morpholinyl)methylphenol (77802-87-0)

Guidance literature:

With copper diacetate; sodium acetate; In toluene; at 80 ℃; for 18h;

DOI:10.1021/jacs.7b06785

Reference yield: 93.0%

morpholine (110-91-8,99108-56-2) + formaldehyd (50-00-0,30525-89-4,61233-19-0) + 4-chloro-phenol (106-48-9,82344-39-6) → 4-chloro-2-(N-morpholinyl)methylphenol (77802-87-0)

Guidance literature:

In benzene; for 6h; Heating;

DOI:10.1016/S0022-328X(99)00148-5

Reference yield: 83.0%

morpholine (110-91-8,99108-56-2) + 4-Chlorophenylboronic acid (1679-18-1) → 4-chloro-2-(N-morpholinyl)methylphenol (77802-87-0)

Guidance literature:

With di-tert-butyl peroxide; In dichloromethane; at 20 ℃; for 8h;

upstream raw materials:

morpholine

formaldehyd

4-chloro-phenol

4-chloro-1,2-quinodimethane

Downstream raw materials:

C₁₃H₁₇BrClNO₂

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