4'-DeMethoxypiperlotine C

Base Information

Chemical Name:4'-DeMethoxypiperlotine C
CAS No.:807372-38-9
Molecular Formula:C₁₅H₁₉NO₃
Molecular Weight:261.321
Hs Code.:
Mol file:807372-38-9.mol

Synonyms:

Suppliers and Price of 4'-DeMethoxypiperlotine C

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
4'-DemethoxypiperlotineC 95+%
5mg
$ 802.00

Total 6 raw suppliers

Chemical Property of 4'-DeMethoxypiperlotine C

Chemical Property:

PSA：38.77000
LogP:2.27730

Purity/Quality:

98%Min ^*data from raw suppliers

4'-DemethoxypiperlotineC 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4'-DeMethoxypiperlotine C

There total 3 articles about 4'-DeMethoxypiperlotine C which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 7311-34-4
3,5-dimethoxybenzaldehdye

: 66932-75-0
diethyl <2-oxo-2-(1-pyrrolidinyl)ethyl>phosphoante

: 807372-38-9
(E)-3-(3,5-dimethoxyphenyl)-1-(pyrrolidin-1-yl)prop-2-en-1-one

Guidance literature:: With potassium carbonate; In acetonitrile; Reflux;
DOI:10.1080/00397911.2018.1550204

Reference yield: 72.0%

: 123-75-1
pyrrolidine

: 201230-82-2
carbon monoxide

: 171290-52-1
1-Ethynyl-3,5-dimethoxy-benzene

: 807372-38-9
(E)-3-(3,5-dimethoxyphenyl)-1-(pyrrolidin-1-yl)prop-2-en-1-one

Guidance literature:: With triiron dodecarbonyl; triethylamine; 1,4-bis(2,6-diisopropylphenyl)-2,3-dimethyl-1,4-diazabuta-1,3-diene; In tetrahydrofuran; at 120 ℃; for 16h; under 7500.75 Torr; regioselective reaction; Autoclave; Inert atmosphere;
DOI:10.1002/anie.201005823

Reference yield:

: 90892-09-4
bromoacetopyrrolidine

: 807372-38-9
(E)-3-(3,5-dimethoxyphenyl)-1-(pyrrolidin-1-yl)prop-2-en-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 4.5 h / 60 °C

2: potassium carbonate / acetonitrile / Reflux

With potassium carbonate; In acetonitrile; 1: |Michaelis-Arbuzov Synthesis / 2: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1080/00397911.2018.1550204