Benzoic acid, 3-(methoxymethoxy)-, methyl ester

Base Information

Chemical Name:Benzoic acid, 3-(methoxymethoxy)-, methyl ester
CAS No.:81245-42-3
Molecular Formula:C10H12O4
Molecular Weight:196.203
Hs Code.:

Synonyms:methyl 3-methoxymethoxy-benzoate;methyl-3-(methoxymethoxy)benzoate;methyl 3-(methoxymethoxy)benzoate;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid, 3-(methoxymethoxy)-, methyl ester

Chemical Property:

PSA：44.76000
LogP:1.45590

Purity/Quality:

Safty Information:

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Hazard Codes:

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Technology Process of Benzoic acid, 3-(methoxymethoxy)-, methyl ester

There total 4 articles about Benzoic acid, 3-(methoxymethoxy)-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 109-87-5
Dimethoxymethane

: 19438-10-9
methyl 3-hydroxybenzoate

: 81245-42-3
methyl 3-{[(methyloxy)methyl]oxy}benzoate

Guidance literature:: With 4 A molecular sieve; toluene-4-sulfonic acid; In dichloromethane; for 24h; Heating;
DOI:10.1021/jo060175c

Reference yield:

: 67-56-1
methanol

: 107-30-2
chloromethyl methyl ether

: 99-06-9
3-Carboxyphenol

: 81245-42-3
methyl 3-{[(methyloxy)methyl]oxy}benzoate

Guidance literature:: methanol; 3-Carboxyphenol; With sulfuric acid;

chloromethyl methyl ether; With potassium carbonate;

Reference yield:

: 99-06-9
3-Carboxyphenol

: 81245-42-3
methyl 3-{[(methyloxy)methyl]oxy}benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / conc. H₂SO₄ / 5 h

2: 66 percent / p-toluenesulfonic acid monohydrate / CH₂Cl₂ / 24 h / Heating

With sulfuric acid; toluene-4-sulfonic acid; In dichloromethane;
DOI:10.1021/jo00132a022