1H-Pyrazol-5-ol, 1-benzoyl-4,5-dihydro-3-methyl-5-phenyl-

Base Information

Chemical Name:1H-Pyrazol-5-ol, 1-benzoyl-4,5-dihydro-3-methyl-5-phenyl-
CAS No.:82366-05-0
Molecular Formula:C17H16N2O2
Molecular Weight:280.326
Hs Code.:
DSSTox Substance ID:DTXSID90385833
Nikkaji Number:J3.106.521F

Synonyms:82366-05-0;1H-Pyrazol-5-ol, 1-benzoyl-4,5-dihydro-3-methyl-5-phenyl-;CBMicro_019950;Oprea1_504240;Oprea1_547272;DTXSID90385833;CCG-8159;STK868228;(5-Hydroxy-3-methyl-5-phenyl-4,5-dihydro-pyrazol-1-yl)-phenyl-methanone;AKOS000610411;AKOS022088697;BIM-0020148.P001;EU-0043458;1-Benzoyl-3-methyl-5-phenyl-2-pyrazoline-5-ol;(5-hydroxy-3-methyl-5-phenyl-4,5-dihydro-1H-pyrazol-1-yl)(phenyl)methanone

Suppliers and Price of 1H-Pyrazol-5-ol, 1-benzoyl-4,5-dihydro-3-methyl-5-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1H-Pyrazol-5-ol, 1-benzoyl-4,5-dihydro-3-methyl-5-phenyl-

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:280.121177757
Heavy Atom Count:21
Complexity:423

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=NN(C(C1)(C2=CC=CC=C2)O)C(=O)C3=CC=CC=C3

Technology Process of 1H-Pyrazol-5-ol, 1-benzoyl-4,5-dihydro-3-methyl-5-phenyl-

There total 1 articles about 1H-Pyrazol-5-ol, 1-benzoyl-4,5-dihydro-3-methyl-5-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 613-94-5
benzoic acid hydrazide

: 93-91-4
1-phenylbutan-1,3-dione

: 82366-05-0
1-benzoyl-5-hydroxy-3-methyl-5-phenyl-2-pyrazoline

Guidance literature:: In methanol;

Reference yield: 82.0%

: 82366-05-0
1-benzoyl-5-hydroxy-3-methyl-5-phenyl-2-pyrazoline

: 141736-91-6
1-benzoyl-3-methyl-5-phenyl-1H-pyrazole

Guidance literature:: With boron trifluoride diethyl etherate; In tetrahydrofuran; at 25 ℃; for 12h;
DOI:10.1016/j.tet.2012.07.046

Reference yield: 81.0%

: 1135-99-5
diphenyltin(IV) dichloride

: 82366-05-0
1-benzoyl-5-hydroxy-3-methyl-5-phenyl-2-pyrazoline

: diphenyl[4-phenyl-2,4-butanedionebenzoylhydrazonate^(2-)]tin(IV)

Guidance literature:: With Et₃N; In methanol; byproducts: Et3N*HCl; a few drops of Et3N added to soln. of ligand in dry MeOH; filtered; soln. of Ph2SnCl2 (1 equiv.) in dry MeOH added slowly to filtrate at room temp.; 30 min; filtered; ppt. washed with petroleum ether; dried in vac.; elem. anal.;
DOI:10.1016/j.jorganchem.2003.09.035