ETHYL N-(2-HYDROXYETHYL)-CARBAMATE

Base Information

• Chemical Name: ETHYL N-(2-HYDROXYETHYL)-CARBAMATE
• CAS No.: 5602-93-7
• Molecular Formula: C5H11 N O3
• Molecular Weight: 133.147
• Hs Code.: 2924199090
• Mol file: 5602-93-7.mol

Synonyms:Carbamicacid, (2-hydroxyethyl)-, ethyl ester (6CI,7CI,8CI,9CI); Ethyl(2-hydroxyethyl)carbamate; Ethyl N-(2-hydroxyethyl)carbamate; N-2-HydroxyethylO-ethyl carbamate; NSC 11805; NSC 64649

Chemical Property of ETHYL N-(2-HYDROXYETHYL)-CARBAMATE

Chemical Property:

• Vapor Pressure: 0.00273mmHg at 25°C
• Melting Point: 87 °C
• Boiling Point: 253.9°Cat760mmHg
• PKA: 11.99±0.46(Predicted)
• Flash Point: 107.4°C
• PSA: 58.56000
• Density: 1.101g/cm³
• LogP: 0.11570

Purity/Quality:

EthylN-(2-Hydroxyethyl)carbamate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ETHYL N-(2-HYDROXYETHYL)-CARBAMATE

There total 1 articles about ETHYL N-(2-HYDROXYETHYL)-CARBAMATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethanolamine (141-43-5) + Diethyl carbonate (105-58-8,76619-83-5) → dimethylenecyclourethane (497-25-6) + ethyl (2-hydroxyethyl)carbamate (5602-93-7)

Guidance literature:

With 1,3-diisobutylimidazolium hydrogen carbonate; at 100 ℃; for 24h;

DOI:10.1002/ejoc.201600550

Reference yield: 97.0%

ethyl (2-hydroxyethyl)carbamate (5602-93-7) + 3,5-dimethylphenyl iodide (22445-41-6) → 3-(3,5-dimethylphenyl)oxazolidine-2-one

Guidance literature:

With copper(l) iodide; 2,2,6,6-tetramethylheptane-3,5-dione; caesium carbonate; In acetonitrile; at 20 - 100 ℃; for 20h;

DOI:10.1021/ol502322c

Reference yield: 95.0%

iodobenzene (591-50-4) + ethyl (2-hydroxyethyl)carbamate (5602-93-7) → N-phenyl-2-oxazolidinone (703-56-0)

Guidance literature:

With copper(l) iodide; 2,2,6,6-tetramethylheptane-3,5-dione; caesium carbonate; In acetonitrile; at 20 - 80 ℃; for 20h; Temperature; Solvent; Reagent/catalyst;

DOI:10.1021/ol502322c

upstream raw materials:

ethanolamine

Diethyl carbonate

Downstream raw materials:

3-Carboethoxy-2-Oxazolidinone

5-Nitro-furaldehyd-2-<2-(2-hydroxy-ethyl)-semicarbazon>,

ethyl N-(2-chloroethyl)carbamate

2-styryl-oxazolidine-3-carboxylic acid ethyl ester