4,4'-DICHLORO-2,2'-BIPYRIDINE N,N'-DIOXIDE

Base Information

Chemical Name:4,4'-DICHLORO-2,2'-BIPYRIDINE N,N'-DIOXIDE
CAS No.:84175-08-6
Molecular Formula:C10H6Cl2N2O2
Molecular Weight:257.07300
Hs Code.:2933399090
Mol file:84175-08-6.mol

Synonyms:4,4'-dichloro-2,2'-bipyridyl-N,N'-dioxide;4,4'-dichloro-2,2'-bipyridine-N,N'-dioxide;

Suppliers and Price of 4,4'-DICHLORO-2,2'-BIPYRIDINE N,N'-DIOXIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
4,4'-DICHLORO-2,2'-BIPYRIDINE-1,1'-DIOXIDE 95.00%
5MG
$ 498.54

Total 4 raw suppliers

Chemical Property of 4,4'-DICHLORO-2,2'-BIPYRIDINE N,N'-DIOXIDE

Chemical Property:

Boiling Point:625.254oC at 760 mmHg
Flash Point:331.942oC
PSA：50.92000
Density:1.5g/cm3
LogP:3.51740

Purity/Quality:

99% ^*data from raw suppliers

4,4'-DICHLORO-2,2'-BIPYRIDINE-1,1'-DIOXIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4,4'-DICHLORO-2,2'-BIPYRIDINE N,N'-DIOXIDE

There total 3 articles about 4,4'-DICHLORO-2,2'-BIPYRIDINE N,N'-DIOXIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 51595-55-2
4,4'-dinitro-2,2'-bipyridyl-N,N'-dioxide

: 84175-08-6
4,4’-dichloro-2,2’-bipyridine-N,N’-dioxide

Guidance literature:: With acetic acid; acetyl chloride; at 100 ℃; for 2h;
DOI:10.1002/ejic.201601403

Reference yield:

: 366-18-7
[2,2]bipyridinyl

: 84175-08-6
4,4’-dichloro-2,2’-bipyridine-N,N’-dioxide

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / aq. H₂O₂; AcOH / 13 h / 70 - 80 °C

2: 52 percent / HNO₃; H₂SO₄/SO₃ / 8 h / 100 °C

3: 80 percent / AcCl; AcOH / 4 h / 100 °C

With sulfuric acid; sulfur trioxide; dihydrogen peroxide; nitric acid; acetic acid; acetyl chloride;
DOI:10.1021/jo052127i

Reference yield:

: 7275-43-6
[2,2']bipyridinyl 1,1'-dioxide

: 84175-08-6
4,4’-dichloro-2,2’-bipyridine-N,N’-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / HNO₃; H₂SO₄/SO₃ / 8 h / 100 °C

2: 80 percent / AcCl; AcOH / 4 h / 100 °C

With sulfuric acid; sulfur trioxide; nitric acid; acetic acid; acetyl chloride;
DOI:10.1021/jo052127i