5-Bromo-2-chloro-N-methoxy-N-methylbenzamide

Base Information

Chemical Name:5-Bromo-2-chloro-N-methoxy-N-methylbenzamide
CAS No.:842136-59-8
Molecular Formula:C9H9BrClNO2
Molecular Weight:278.533
Hs Code.:2924299090
DSSTox Substance ID:DTXSID40697413
Wikidata:Q82627308
Mol file:842136-59-8.mol

Synonyms:5-BROMO-2-CHLORO-N-METHOXY-N-METHYLBENZAMIDE;842136-59-8;N-Methoxy-N-methyl 5-bromo-2-chlorobenzamide;N-methoxy-N-methyl-5-bromo-2-chlorobenzamide;5-bromo-2-chloro-N-methoxy-N-methyl-benzamide;SCHEMBL153277;DTXSID40697413;VUXHGIZYRNNOSE-UHFFFAOYSA-N;MFCD11847367;AKOS008917017;BS-25889;CS-0209917;FT-0711450;F30185;F1903-0137

Suppliers and Price of 5-Bromo-2-chloro-N-methoxy-N-methylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
N-Methoxy-N-methyl5-bromo-2-chlorobenzamide
100mg
$ 45.00

Crysdot
5-Bromo-2-chloro-N-methoxy-N-methylbenzamide 95+%
10g
$ 355.00

Crysdot
5-Bromo-2-chloro-N-methoxy-N-methylbenzamide 95+%
25g
$ 640.00

American Custom Chemicals Corporation
5-BROMO-2-CHLORO-N-METHOXY-N-METHYLBENZAMIDE 95.00%
5MG
$ 498.15

Alichem
5-Bromo-2-chloro-N-methoxy-N-methylbenzamide
25g
$ 633.08

AK Scientific
N-Methoxy-N-methyl5-bromo-2-chlorobenzamide
25g
$ 957.00

Total 3 raw suppliers

Chemical Property of 5-Bromo-2-chloro-N-methoxy-N-methylbenzamide

Chemical Property:

PSA：29.54000
LogP:2.73590
XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:276.95052
Heavy Atom Count:14
Complexity:215

Purity/Quality:

99% ^*data from raw suppliers

N-Methoxy-N-methyl5-bromo-2-chlorobenzamide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C(=O)C1=C(C=CC(=C1)Br)Cl)OC

Technology Process of 5-Bromo-2-chloro-N-methoxy-N-methylbenzamide

There total 4 articles about 5-Bromo-2-chloro-N-methoxy-N-methylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 21900-52-7
5-bromo-2-chloro-benzoyl chloride

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 842136-59-8
5-bromo-2-chloro-N-methoxy-N-methyl-benzamide

Guidance literature:: N,O-dimethylhydroxylamine*hydrochloride; With triethylamine; In dichloromethane; at -10 - 10 ℃; for 0.5h;

5-bromo-2-chloro-benzoyl chloride; In dichloromethane; for 3h;

Reference yield: 84.0%

: 21739-92-4
5-bromo-2-chlorobenzoic acid

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 842136-59-8
5-bromo-2-chloro-N-methoxy-N-methyl-benzamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃; for 14h;

Reference yield: 76.9%

: 21739-92-4
5-bromo-2-chlorobenzoic acid

: 16645-06-0
N,N-dimethylhydroxylamine hydrochloride

: 842136-59-8
5-bromo-2-chloro-N-methoxy-N-methyl-benzamide

Guidance literature:: N,N-dimethylhydroxylamine hydrochloride; With triethylamine; In dichloromethane; for 16h;

5-bromo-2-chlorobenzoic acid; With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; In dichloromethane;