2-(2-Chlorophenoxy)-2-phenylacetohydrazide

Base Information

• Chemical Name: 2-(2-Chlorophenoxy)-2-phenylacetohydrazide
• CAS No.: 32191-72-3
• Molecular Formula: C₁₄H₁₃ClN₂O₂
• Molecular Weight: 276.722
• NSC Number: 107366
• DSSTox Substance ID: DTXSID90296056
• Mol file: 32191-72-3.mol

Synonyms:2-(2-chlorophenoxy)-2-phenylacetohydrazide;32191-72-3;NSC107366;DTXSID90296056;AKOS012885392;NSC-107366

Chemical Property of 2-(2-Chlorophenoxy)-2-phenylacetohydrazide

Chemical Property:

• Vapor Pressure: 3.1E-10mmHg at 25°C
• Boiling Point: 502.7°Cat760mmHg
• Flash Point: 257.8°C
• Density: 1.299g/cm³
• XLogP3: 2.8
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 276.0665554
• Heavy Atom Count: 19
• Complexity: 295

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(C(=O)NN)OC2=CC=CC=C2Cl

Technology Process of 2-(2-Chlorophenoxy)-2-phenylacetohydrazide

There total 3 articles about 2-(2-Chlorophenoxy)-2-phenylacetohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 2-(2-chlorophenoxy)-2-phenylacetate (32191-47-2) → (2-Chloro-phenoxy)-phenyl-acetic acid hydrazide (32191-72-3)

Guidance literature:

With hydrazine hydrate;

Reference yield:

bromo-phenyl-acetic acid methyl ester (37167-62-7,3042-81-7,61139-20-6) → (2-Chloro-phenoxy)-phenyl-acetic acid hydrazide (32191-72-3)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃

2: N₂H₄*H₂O

With potassium carbonate; hydrazine hydrate;

Reference yield:

2-monochlorophenol (95-57-8) → (2-Chloro-phenoxy)-phenyl-acetic acid hydrazide (32191-72-3)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃

2: N₂H₄*H₂O

With potassium carbonate; hydrazine hydrate;

upstream raw materials:

methyl 2-(2-chlorophenoxy)-2-phenylacetate

bromo-phenyl-acetic acid methyl ester

2-monochlorophenol

Downstream raw materials:

Dichloro-acetic acid N'-[2-(2-chloro-phenoxy)-2-phenyl-acetyl]-hydrazide

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