Acetamide, N-[1-[[4-(aminoiminomethyl)phenyl]methyl]-2-(4-morpholinyl)-2-oxoethyl] -2-[[(4-methylphenyl)sulfonyl]amino]-, monohydrochloride

Base Information

Chemical Name:Acetamide, N-[1-[[4-(aminoiminomethyl)phenyl]methyl]-2-(4-morpholinyl)-2-oxoethyl] -2-[[(4-methylphenyl)sulfonyl]amino]-, monohydrochloride
CAS No.:84792-56-3
Molecular Formula:C23H29N5O5S.ClH
Molecular Weight:524.041
Hs Code.:

Acetamide,
N-[1-[[4-(aminoiminomethyl)phenyl]methyl]-2-(4-morpholinyl)-2-oxoethyl]
-2-[[(4-methylphenyl)sulfonyl]amino]-, monohydrochloride

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Chemical Property of Acetamide, N-[1-[[4-(aminoiminomethyl)phenyl]methyl]-2-(4-morpholinyl)-2-oxoethyl] -2-[[(4-methylphenyl)sulfonyl]amino]-, monohydrochloride

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Technology Process of Acetamide, N-[1-[[4-(aminoiminomethyl)phenyl]methyl]-2-(4-morpholinyl)-2-oxoethyl] -2-[[(4-methylphenyl)sulfonyl]amino]-, monohydrochloride

There total 8 articles about Acetamide, N-[1-[[4-(aminoiminomethyl)phenyl]methyl]-2-(4-morpholinyl)-2-oxoethyl] -2-[[(4-methylphenyl)sulfonyl]amino]-, monohydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 84792-55-2
4-{3-Morpholin-4-yl-3-oxo-2-[2-(toluene-4-sulfonylamino)-acetylamino]-propyl}-benzimidic acid methyl ester; hydrochloride

: 84792-56-3
N_α-(Tosylglycyl)-4-amidinophenylalaninmorpholidhydrochlorid

Guidance literature:: With ammonia; In methanol; at 60 ℃; for 3h;

Reference yield:

: 52117-01-8
N-acetyl-4-cyano-α-(ethoxycarbonyl)phenylalanine ethyl ester

: 84792-56-3
N_α-(Tosylglycyl)-4-amidinophenylalaninmorpholidhydrochlorid

Guidance literature:: Multi-step reaction with 6 steps

1: NaOH (1 mol/l) / acetic acid; H₂O / pH 3.8-4.0

2: NaOH (1 mol/l) / diethyl ether; ethyl acetate; H₂O / 10 h

3: 60 percent / DCC / pyridine / 12 h / Ambient temperature

4: 40 percent / pyridine; dimethylformamide / 7 h / Ambient temperature

5: 80 percent / HCl-gas in abs.MeOH (1,0 g/2ml) / dioxane; methanol / 48 h / 5 °C

6: 70 percent / NH₃ / methanol / 3 h / 60 °C

With hydrogenchloride; sodium hydroxide; ammonia; dicyclohexyl-carbodiimide; In 1,4-dioxane; pyridine; methanol; diethyl ether; water; acetic acid; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 56218-62-3
2-(4-methylphenylsulfonamido)acetyl chloride

: 84792-56-3
N_α-(Tosylglycyl)-4-amidinophenylalaninmorpholidhydrochlorid

Guidance literature:: Multi-step reaction with 5 steps

1: NaOH (1 mol/l) / diethyl ether; ethyl acetate; H₂O / 10 h

2: 60 percent / DCC / pyridine / 12 h / Ambient temperature

3: 40 percent / pyridine; dimethylformamide / 7 h / Ambient temperature

4: 80 percent / HCl-gas in abs.MeOH (1,0 g/2ml) / dioxane; methanol / 48 h / 5 °C

5: 70 percent / NH₃ / methanol / 3 h / 60 °C

With hydrogenchloride; sodium hydroxide; ammonia; dicyclohexyl-carbodiimide; In 1,4-dioxane; pyridine; methanol; diethyl ether; water; ethyl acetate; N,N-dimethyl-formamide;