(6Z)-6-[(propylamino)methylidene]cyclohexa-2,4-dien-1-one - copper (2:1)

Base Information

Chemical Name:(6Z)-6-[(propylamino)methylidene]cyclohexa-2,4-dien-1-one - copper (2:1)
CAS No.:14077-15-7
Molecular Formula:C₂₀H₂₄CuN₂O₂
Molecular Weight:387.969
Hs Code.:

Synonyms:Copper,bis[2-[(propylimino)methyl]phenolato-N,O]-; Copper,bis[o-(N-propylformimidoyl)phenolato]- (6CI,7CI,8CI); Phenol,2-[(propylimino)methyl]-, copper complex;Bis(N-propylsalicylideneaminato)copper; Bis(propylsalicylaldimine)copper(II);NSC 124653

Suppliers and Price of (6Z)-6-[(propylamino)methylidene]cyclohexa-2,4-dien-1-one - copper (2:1)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of (6Z)-6-[(propylamino)methylidene]cyclohexa-2,4-dien-1-one - copper (2:1)

Chemical Property:

Vapor Pressure:0.00289mmHg at 25°C
Boiling Point:284.9°C at 760 mmHg
Flash Point:120°C

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (6Z)-6-[(propylamino)methylidene]cyclohexa-2,4-dien-1-one - copper (2:1)

There total 5 articles about (6Z)-6-[(propylamino)methylidene]cyclohexa-2,4-dien-1-one - copper (2:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 32382-63-1,146305-09-1
N-n-propylsalicylideneamine

: 6046-93-1
copper(II) acetate monohydrate

: 37703-49-4,14077-15-7
bis[N-n-propyl-2-oxy-κO-benzylidenimine-κN-(1–)]copper(II)

Guidance literature:: In ethanol; for 2.5h; Reflux;
DOI:10.1016/j.ica.2021.120460

Reference yield:

: 107-10-8,42939-71-9
propylamine

: 14523-25-2,43190-54-1,86195-53-1
{Cusal₂}

: 37703-49-4,14077-15-7
bis[N-n-propyl-2-oxy-κO-benzylidenimine-κN-(1–)]copper(II)

Guidance literature:: In ethanol; reflux;; recrystn. from CHCl3-alc.;;
DOI:10.1021/ja01489a014

Reference yield:

: 107-10-8,42939-71-9
propylamine

: 142-71-2
copper diacetate

: 90-02-8
salicylaldehyde

: 37703-49-4,14077-15-7
bis[N-n-propyl-2-oxy-κO-benzylidenimine-κN-(1–)]copper(II)

Guidance literature:: With NaOOCCH₃*3H₂O; In methanol; water; addn. of 0.1 mol C3H7NH2 to a soln. of 0.05 mol salicylaldehyde in methanol; successive addn. of an aq. soln. of Cu(II)-acetate and an aq. soln. of NaOOCCH3*3H2O; heating for 15-30 minutes under stirring;; sucking off; recrystn. from methanol; drying in vac. over CaCl2;;
DOI:10.1021/jo01357a025