Aziridine, 1-[(2,4-dimethoxyphenyl)methyl]-2-ethenyl-

Base Information

Chemical Name:Aziridine, 1-[(2,4-dimethoxyphenyl)methyl]-2-ethenyl-
CAS No.:848645-61-4
Molecular Formula:C13H17NO2
Molecular Weight:219.283
Hs Code.:

Synonyms:

Suppliers and Price of Aziridine, 1-[(2,4-dimethoxyphenyl)methyl]-2-ethenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Aziridine, 1-[(2,4-dimethoxyphenyl)methyl]-2-ethenyl-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Aziridine, 1-[(2,4-dimethoxyphenyl)methyl]-2-ethenyl-

There total 5 articles about Aziridine, 1-[(2,4-dimethoxyphenyl)methyl]-2-ethenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1779-49-3
Methyltriphenylphosphonium bromide

: 848645-69-2
1-(2,4-dimethoxybenzyl)aziridine-2-carbaldehyde

: 848645-61-4
1-(2,4-dimethoxybenzyl)-2-vinylaziridine

Guidance literature:: With potassium hexamethylsilazane; In tetrahydrofuran; at -15 - 20 ℃;
DOI:10.1021/ol047513l

Reference yield: 62.0%

: 2065-66-9
methyl-triphenylphosphonium iodide

: 848645-69-2
1-(2,4-dimethoxybenzyl)aziridine-2-carbaldehyde

: 848645-61-4
1-(2,4-dimethoxybenzyl)-2-vinylaziridine

Guidance literature:: methyl-triphenylphosphonium iodide; With sodium hexamethyldisilazane; In tetrahydrofuran; at 0 - 20 ℃; for 0.5h; Inert atmosphere;

1-(2,4-dimethoxybenzyl)aziridine-2-carbaldehyde; In tetrahydrofuran; at -10 - 20 ℃; for 6h; Inert atmosphere;
DOI:10.1039/c8ob03029d

Reference yield:

: 848645-68-1
1-(2,4-dimethoxybenzyl)aziridine-2-carboxylic acid ethyl ester

: 848645-61-4
1-(2,4-dimethoxybenzyl)-2-vinylaziridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: DIBAL-H / hexane; CH₂Cl₂ / 1.5 h / -78 °C

1.2: aq. NaF / hexane; CH₂Cl₂ / 0.83 h / -78 - 20 °C

2.1: 76 percent / KHMDS / tetrahydrofuran / -15 - 20 °C

With potassium hexamethylsilazane; diisobutylaluminium hydride; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ol047513l