Carbamic acid, [(5S)-5-[[(1,1-dimethylethoxy)carbonyl]amino]-6-[[4-[[[(1,1-dimethylethyl) dimethylsilyl]oxy]methyl]phenyl]amino]-6-oxohexyl]-, 2-propenyl ester

Base Information

Chemical Name:Carbamic acid, [(5S)-5-[[(1,1-dimethylethoxy)carbonyl]amino]-6-[[4-[[[(1,1-dimethylethyl) dimethylsilyl]oxy]methyl]phenyl]amino]-6-oxohexyl]-, 2-propenyl ester
CAS No.:848824-85-1
Molecular Formula:C28H47N3O6Si
Molecular Weight:549.783
Hs Code.:

Carbamic acid,
[(5S)-5-[[(1,1-dimethylethoxy)carbonyl]amino]-6-[[4-[[[(1,1-dimethylethyl)
dimethylsilyl]oxy]methyl]phenyl]amino]-6-oxohexyl]-, 2-propenyl ester

Synonyms:

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Chemical Property of Carbamic acid, [(5S)-5-[[(1,1-dimethylethoxy)carbonyl]amino]-6-[[4-[[[(1,1-dimethylethyl) dimethylsilyl]oxy]methyl]phenyl]amino]-6-oxohexyl]-, 2-propenyl ester

Chemical Property:

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Safty Information:

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MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamic acid, [(5S)-5-[[(1,1-dimethylethoxy)carbonyl]amino]-6-[[4-[[[(1,1-dimethylethyl) dimethylsilyl]oxy]methyl]phenyl]amino]-6-oxohexyl]-, 2-propenyl ester

There total 3 articles about Carbamic acid, [(5S)-5-[[(1,1-dimethylethoxy)carbonyl]amino]-6-[[4-[[[(1,1-dimethylethyl) dimethylsilyl]oxy]methyl]phenyl]amino]-6-oxohexyl]-, 2-propenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 848824-84-0
[5-tert-butoxycarbonylamino-5-(4-hydroxymethylphenylcarbamoyl)pentyl]-carbamic acid allyl ester

: 848824-85-1
{5-allyloxycarbonylamino-1-[4-(tert-butyl-dimethyl-silanyloxymethyl)phenylcarbamoyl]-pentyl}-carbamic acid tert-butyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 0.166667h;
DOI:10.1021/jm040137q

Reference yield:

: 623-04-1
4-aminobenzenemethanol

: 848824-85-1
{5-allyloxycarbonylamino-1-[4-(tert-butyl-dimethyl-silanyloxymethyl)phenylcarbamoyl]-pentyl}-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / EEDQ / CHCl₃ / 2 h / 20 °C

2: 87 percent / DIPEA / dimethylformamide / 0.17 h

With N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; N-ethyl-N,N-diisopropylamine; In chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jm040137q

Reference yield:

: 104669-73-0
N^α-(tert-butoxycarbonyl)-N^ε-(allyloxycarbonyl)-L-lysine

: 848824-85-1
{5-allyloxycarbonylamino-1-[4-(tert-butyl-dimethyl-silanyloxymethyl)phenylcarbamoyl]-pentyl}-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / EEDQ / CHCl₃ / 2 h / 20 °C

2: 87 percent / DIPEA / dimethylformamide / 0.17 h

With N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; N-ethyl-N,N-diisopropylamine; In chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jm040137q