CYCLOHEXYL CARBANILATE

Base Information

• Chemical Name: CYCLOHEXYL CARBANILATE
• CAS No.: 3770-95-4
• Molecular Formula: C13H17NO2
• Molecular Weight: 219.283
• Hs Code.: 2924299090
• Mol file: 3770-95-4.mol

Synonyms:cyclohexyl N-phenylcarbamate;CYCLOHEXYL CARBANILATE;

Chemical Property of CYCLOHEXYL CARBANILATE

Chemical Property:

• Vapor Pressure: 0.00145mmHg at 25°C
• Melting Point: 85-86℃
• Boiling Point: 296.3°Cat760mmHg
• Flash Point: 133°C
• PSA: 38.33000
• Density: 1.1g/cm³
• LogP: 3.64080
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

CYCLOHEXYL CARBANILATE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of CYCLOHEXYL CARBANILATE

There total 26 articles about CYCLOHEXYL CARBANILATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

tert-butyl phenylcarbamate (3422-01-3) + cyclohexanol (108-93-0) → O-cyclohexyl N-phenylcarbamate (3770-95-4)

Guidance literature:

With cobalt(II) iodide; zinc; tris(p-dimethylaminophenyl)phosphine; In toluene; at 120 ℃; for 28h; Schlenk technique; Inert atmosphere; Glovebox;

DOI:10.1039/c9ob00924h

Reference yield: 95.0%

phenyl isocyanate (103-71-9) + cyclohexanol (108-93-0) → O-cyclohexyl N-phenylcarbamate (3770-95-4)

Guidance literature:

With MoCl₂O₂(dmf)2; In dichloromethane; at 20 ℃; for 0.333333h;

DOI:10.1055/s-0030-1258552

Reference yield: 94.0%

carbon monoxide (201230-82-2) + nitrobenzene (98-95-3,26969-40-4) + cyclohexanol (108-93-0) → O-cyclohexyl N-phenylcarbamate (3770-95-4)

Guidance literature:

With pyridine; iron(III) chloride; palladium dichloride; at 165 ℃; for 2.5h; under 75005.9 Torr; Product distribution; var. temp., pressure and time; other aromatic nitro compounds;

DOI:10.1007/BF01172272

upstream raw materials:

phenyl isocyanate

cyclohexanol

aniline

urea

Downstream raw materials:

4-nitrophenylcarbamic acid cyclohexyl ester

cyclohexyl N-(4-aminophenyl)carbamate

(4-nitroso-phenyl)-carbamic acid cyclohexyl ester