4,4'-[Methylenebis(oxy)]diphenol

Base Information

Chemical Name:4,4'-[Methylenebis(oxy)]diphenol
CAS No.:86072-79-9
Molecular Formula:C13H12O4
Molecular Weight:232.236
Hs Code.:
DSSTox Substance ID:DTXSID60579803
Nikkaji Number:J2.950.193I
Wikidata:Q82470427

Synonyms:4,4'-[Methylenebis(oxy)]diphenol;86072-79-9;SCHEMBL8452874;DTXSID60579803

Suppliers and Price of 4,4'-[Methylenebis(oxy)]diphenol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 4,4'-[Methylenebis(oxy)]diphenol

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:232.07355886
Heavy Atom Count:17
Complexity:184

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1O)OCOC2=CC=C(C=C2)O

Technology Process of 4,4'-[Methylenebis(oxy)]diphenol

There total 3 articles about 4,4'-[Methylenebis(oxy)]diphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 142746-15-4
bis(4-(benzyloxy)phenoxy)methane

: 86072-79-9
bis(4-hydroxyphenoxy)methane

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; under 760 Torr; Ambient temperature;
DOI:10.1021/jo00046a038

Reference yield: 91.0%

: 75-09-2
dichloromethane

: 103-16-2
4-Benzyloxyphenol

: 86072-79-9
bis(4-hydroxyphenoxy)methane

Guidance literature:: dichloromethane; 4-Benzyloxyphenol; With tetrabutylammomium bromide; potassium hydroxide; at 20 ℃; for 40h;

With palladium 10% on activated carbon; hydrogen; In ethyl acetate; at 20 ℃; under 760.051 Torr;
DOI:10.1021/jo2000397

Reference yield:

: 103-16-2
4-Benzyloxyphenol

: 86072-79-9
bis(4-hydroxyphenoxy)methane

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / KOH / TBAB / 40 h / Ambient temperature

2: 96 percent / H₂ / 10percent Pd/C / ethyl acetate / 760 Torr / Ambient temperature

With potassium hydroxide; hydrogen; palladium on activated charcoal; tetrabutylammomium bromide; In ethyl acetate;
DOI:10.1021/jo00046a038