7-BROMO-3-PHENYL-2-QUINOLINOL

Base Information

• Chemical Name: 7-BROMO-3-PHENYL-2-QUINOLINOL
• CAS No.: 861872-50-6
• Molecular Formula: C15H10BrNO
• Molecular Weight: 300.154
• Hs Code.: 2933790090
• Mol file: 861872-50-6.mol

Synonyms:7-Bromo-3-phenyl-quinolin-2-ol;7-BROMO-3-PHENYL-2-QUINOLINOL;7-Bromo-2-hydroxy-3-phenylquinoline;7-Bromo-3-phenylquinolin-2(1H)-one;

Chemical Property of 7-BROMO-3-PHENYL-2-QUINOLINOL

Chemical Property:

• Vapor Pressure: 2.7E-09mmHg at 25°C
• Boiling Point: 465.7oC at 760 mmHg
• Flash Point: 235.5oC
• PSA: 33.12000
• Density: 1.526g/cm3
• LogP: 4.36990
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

7-Bromo-2-hydroxy-3-phenylquinoline ^*data from reagent suppliers

Safty Information:

• Statements: 41
• Safety Statements: 26-39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 7-BROMO-3-PHENYL-2-QUINOLINOL

There total 1 articles about 7-BROMO-3-PHENYL-2-QUINOLINOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(3-bromophenyl)-α-(phenylmethylene)benzeneacetamide → C15H10BrNO (861872-50-6) + C15H10BrNO (1207982-16-8)

Guidance literature:

With aluminum (III) chloride; In chlorobenzene; at 20 ℃; for 3h; Heating / reflux;

Reference yield: 88.0%

methanol (67-56-1) + carbon monoxide (201230-82-2) + 7-bromo-3-phenyl-2-quinolinol (861872-50-6) → methyl 2-hydroxy-3-phenylquinoline-7-carboxylate (1383849-47-5)

Guidance literature:

With sodium acetate; palladium diacetate; triphenylphosphine; In N,N-dimethyl-formamide; at 80 ℃; under 5171.62 Torr;

Reference yield:

C15H10BrNO (861872-50-6) + C15H10BrNO (1207982-16-8) → 7-bromo-2-chloro-3-phenylquinoline (85274-44-8) + C15H9BrClN (861872-51-7)

Guidance literature:

With trichlorophosphate; for 1h; Heating / reflux;

Downstream raw materials:

7-bromo-2-chloro-3-phenylquinoline

C₁₅H₉BrClN

methyl 2-hydroxy-3-phenylquinoline-7-carboxylate

C₂₅H₂₇NO₄

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