Carbonochloridic acid, 2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl ester

Base Information

• Chemical Name: Carbonochloridic acid, 2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl ester
• CAS No.: 866-02-4
• Molecular Formula: C8H3ClF12O2
• Molecular Weight: 394.54200

Synonyms:1H,1H,7H-Dodecafluorheptylchloroformat;1H,1H,7H-Dodecafluorheptyl-chloroformat;<1,1,7-Trihydro-perfluor-heptyl>-chlorocarbonat;

Chemical Property of Carbonochloridic acid, 2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl ester

Chemical Property:

• Boiling Point: 63 °C(Press: 3 Torr)
• PSA: 26.30000
• Density: 1.7240 g/cm3
• LogP: 4.80340

Purity/Quality:

95% ^*data from raw suppliers

1H,1H,7H-Perfluoroheptyl chloroformate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Carbonochloridic acid, 2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl ester

There total 3 articles about Carbonochloridic acid, 2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

phosgene (75-44-5) + 2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoro-1-heptanol (335-99-9) → 1H,1H,7H-Dodecafluorheptyl-chloroformat (866-02-4)

Guidance literature:

With N,N-dimethyl-formamide; at 90 ℃; for 2.5h;

DOI:10.1134/S1070363208050289

Reference yield:

tetrachloromethane (56-23-5) + 2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoro-1-heptanol (335-99-9) → 1H,1H,7H-Dodecafluorheptyl-chloroformat (866-02-4)

Guidance literature:

With water; iron(III) chloride;

DOI:10.1021/jo01013a025

Reference yield:

→ 1H,1H,7H-Dodecafluorheptyl-chloroformat (866-02-4)

Guidance literature:

Aus Phosgen u. 1H,1H,7H-Dodecafluor-1-heptanol;

upstream raw materials:

tetrachloromethane

2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoro-1-heptanol

phosgene

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