Ethanethioic acid, S-[[bis(4-chlorophenyl)phosphinyl]methyl] ester

Base Information

Chemical Name:Ethanethioic acid, S-[[bis(4-chlorophenyl)phosphinyl]methyl] ester
CAS No.:866363-66-8
Molecular Formula:C15H13Cl2O2PS
Molecular Weight:359.213
Hs Code.:
DSSTox Substance ID:DTXSID10469765
Wikidata:Q82297619

Synonyms:866363-66-8;S-((Bis(4-chlorophenyl)phosphoryl)methyl) ethanethioate;Ethanethioic acid, S-[[bis(4-chlorophenyl)phosphinyl]methyl] ester;DTXSID10469765

Suppliers and Price of Ethanethioic acid, S-[[bis(4-chlorophenyl)phosphinyl]methyl] ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Ethanethioic acid, S-[[bis(4-chlorophenyl)phosphinyl]methyl] ester

Chemical Property:

XLogP3:4.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:357.9750932
Heavy Atom Count:21
Complexity:377

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)SCP(=O)(C1=CC=C(C=C1)Cl)C2=CC=C(C=C2)Cl

Technology Process of Ethanethioic acid, S-[[bis(4-chlorophenyl)phosphinyl]methyl] ester

There total 2 articles about Ethanethioic acid, S-[[bis(4-chlorophenyl)phosphinyl]methyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 873-77-8
(4-chlorphenyl)magnesium bromide

: 866363-66-8
thioacetic acid S-{[di-(4-chlorophenyl)phosphanyl oxide]methyl}ester

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 24 h / Heating

2: dimethylformamide

In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo0620056

Reference yield:

: 13685-36-4
Bis-(p-chlorphenyl)-chlormethylphosphinoxid

: 10387-40-3
potassium thioacetate

: 866363-66-8
thioacetic acid S-{[di-(4-chlorophenyl)phosphanyl oxide]methyl}ester

Guidance literature:: In tetrahydrofuran; Heating;
DOI:10.1021/jo0505472

Reference yield: 53.0%

: 866363-66-8
thioacetic acid S-{[di-(4-chlorophenyl)phosphanyl oxide]methyl}ester

: 108-55-4
glutaric anhydride,

: 866363-67-9
4-carboxythiobutyric acid S-{[di-(4-chlorophenyl)phosphanyl oxide]methyl}ester

Guidance literature:: thioacetic acid S-{[di-(4-chlorophenyl)phosphanyl oxide]methyl}ester; With sodium methylate; In N,N-dimethyl-formamide; at 0 ℃; for 2h;

glutaric anhydride,; In N,N-dimethyl-formamide; at 0 ℃; for 0.333333h;
DOI:10.1021/jo0505472