4-carboxythiobutyric acid S-{[di-(4-chlorophenyl)phosphanyl]methyl}ester

Base Information

Chemical Name:4-carboxythiobutyric acid S-{[di-(4-chlorophenyl)phosphanyl]methyl}ester
CAS No.:866363-68-0
Molecular Formula:C₁₈H₁₇Cl₂O₃PS
Molecular Weight:415.277
Hs Code.:

Synonyms:4-carboxythiobutyric acid S-{[di-(4-chlorophenyl)phosphanyl]methyl}ester

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Chemical Property of 4-carboxythiobutyric acid S-{[di-(4-chlorophenyl)phosphanyl]methyl}ester

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Technology Process of 4-carboxythiobutyric acid S-{[di-(4-chlorophenyl)phosphanyl]methyl}ester

There total 4 articles about 4-carboxythiobutyric acid S-{[di-(4-chlorophenyl)phosphanyl]methyl}ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 866363-67-9
4-carboxythiobutyric acid S-{[di-(4-chlorophenyl)phosphanyl oxide]methyl}ester

: 866363-68-0
4-carboxythiobutyric acid S-{[di-(4-chlorophenyl)phosphanyl]methyl}ester

Guidance literature:: With trichlorosilane; In 1,2-dichloro-ethane; for 72h;
DOI:10.1021/jo0505472

Reference yield:

: 866363-66-8
thioacetic acid S-{[di-(4-chlorophenyl)phosphanyl oxide]methyl}ester

: 866363-68-0
4-carboxythiobutyric acid S-{[di-(4-chlorophenyl)phosphanyl]methyl}ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaOMe / dimethylformamide / 2 h / 0 °C

1.2: 53 percent / dimethylformamide / 0.33 h / 0 °C

2.1: 51 percent / HSiCl₃ / 1,2-dichloro-ethane / 72 h

With trichlorosilane; sodium methylate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/jo0505472

Reference yield:

: 13685-36-4
Bis-(p-chlorphenyl)-chlormethylphosphinoxid

: 866363-68-0
4-carboxythiobutyric acid S-{[di-(4-chlorophenyl)phosphanyl]methyl}ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 2.1 g / tetrahydrofuran / Heating

2.1: NaOMe / dimethylformamide / 2 h / 0 °C

2.2: 53 percent / dimethylformamide / 0.33 h / 0 °C

3.1: 51 percent / HSiCl₃ / 1,2-dichloro-ethane / 72 h

With trichlorosilane; sodium methylate; In tetrahydrofuran; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/jo0505472