2-Propen-1-one, 1-phenyl-3-(2,4,6-trimethylphenyl)-, (2E)-

Base Information

Chemical Name:2-Propen-1-one, 1-phenyl-3-(2,4,6-trimethylphenyl)-, (2E)-
CAS No.:87172-18-7
Molecular Formula:C18H18O
Molecular Weight:250.33500
Hs Code.:
Mol file:87172-18-7.mol

Synonyms:(E)-1-Phenyl-3-(2,4,6-trimethyl-phenyl)-propenone;(E)-3-mesityl-1-phenylprop-2-en-1-one;2,4,6-Trimethyl-trans-chalkon;2,4,6-trimethyl-trans-chalcone;(E)-3-(2,4,6-trimethylphenyl)-1-phenyl-2-propen-1-one;(E)-1-phenyl-3-(2,4,6-trimethylphenyl)prop-2-en-1-one;

Suppliers and Price of 2-Propen-1-one, 1-phenyl-3-(2,4,6-trimethylphenyl)-, (2E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
(2E)-3-Mesityl-1-phenylprop-2-en-1-one
500mg
$ 158.00

American Custom Chemicals Corporation
(2E)-3-MESITYL-1-PHENYLPROP-2-EN-1-ONE 95.00%
5G
$ 1155.00

American Custom Chemicals Corporation
(2E)-3-MESITYL-1-PHENYLPROP-2-EN-1-ONE 95.00%
1G
$ 693.00

American Custom Chemicals Corporation
(2E)-3-MESITYL-1-PHENYLPROP-2-EN-1-ONE 95.00%
0.5G
$ 638.00

Total 4 raw suppliers

Chemical Property of 2-Propen-1-one, 1-phenyl-3-(2,4,6-trimethylphenyl)-, (2E)-

Chemical Property:

Melting Point:101 - 103 °C (ethanol)
PSA：17.07000
LogP:4.50790

Purity/Quality:

98%min ^*data from raw suppliers

(2E)-3-Mesityl-1-phenylprop-2-en-1-one ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-Propen-1-one, 1-phenyl-3-(2,4,6-trimethylphenyl)-, (2E)-

There total 5 articles about 2-Propen-1-one, 1-phenyl-3-(2,4,6-trimethylphenyl)-, (2E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 487-68-3
mesytaldehyde

: 98-86-2
acetophenone

: 87172-18-7
(E)-1-phenyl-3-[(2,4,6-trimethylphenyl)]prop-2-en-1-one

Guidance literature:: mesytaldehyde; acetophenone; With potassium hydroxide; In ethanol; water; at 20 ℃; for 12h;

With hydrogenchloride; In ethanol; water; pH=3 - 4;
DOI:10.1016/j.bmc.2009.02.052

Reference yield: 67.0%

: 487-68-3
mesytaldehyde

: 74636-46-7
C₈H₆LiO^(1-)*Li⁽¹⁺⁾

: 87172-18-7
(E)-1-phenyl-3-[(2,4,6-trimethylphenyl)]prop-2-en-1-one

Guidance literature:: In diethyl ether; -78 deg C -> 0 deg C;
DOI:10.1021/ja00370a073

Reference yield:

: 66057-05-4
(E)- and (Z)-2-bromo-1-phenylethylene acetate

: 87172-18-7
(E)-1-phenyl-3-[(2,4,6-trimethylphenyl)]prop-2-en-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) methyllithium, 2.) tert-butyllithium / 1.) ether, 0 deg C, 2.) -78 -> 0 deg C

2: 67 percent / diethyl ether / -78 deg C -> 0 deg C

With methyllithium; tert.-butyl lithium; In diethyl ether;
DOI:10.1021/ja00370a073