methyl 2,3-dihydroxypropanoate

Base Information

• Chemical Name: methyl 2,3-dihydroxypropanoate
• CAS No.: 15909-76-9
• Molecular Formula: C₄H₈O₄
• Molecular Weight: 120.105
• Mol file: 15909-76-9.mol

Synonyms:Glycericacid, methyl ester (7CI,8CI); 2,3-Dihydroxypropanoic acid methyl ester; Methyl2,3-dihydroxypropionate; Methyl DL-glycerate; Methyl glycerate

Chemical Property of methyl 2,3-dihydroxypropanoate

Chemical Property:

• Vapor Pressure: 0.00616mmHg at 25°C
• Boiling Point: 241.5°Cat760mmHg
• Flash Point: 103.7°C
• Density: 1.285g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl 2,3-dihydroxypropanoate

There total 36 articles about methyl 2,3-dihydroxypropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methyl (R)-2,2-dimethyl-1,3-dioxolane-4-carboxylate (52373-72-5) → methyl (2R)-2,3-dihydroxypropanoate (18289-89-9,15909-76-9)

Guidance literature:

With acetic acid; for 120h; Ambient temperature;

DOI:10.1021/jm00095a019

Reference yield: 100.0%

methyl (4S)-2,2-dimethyl-1,3-dioxolane-4-carboxylate (60456-21-5) → methyl L-glycerate (10303-88-5,15909-76-9)

Guidance literature:

With hydrogenchloride; methanol; for 1h; Ambient temperature;

DOI:10.1016/S0040-4039(00)95704-6

Reference yield: 99.0%

methanol (67-56-1) + glyceric acid (473-81-4,118916-26-0) → methyl glycerate (615-34-9,15909-76-9)

Guidance literature:

With toluene-4-sulfonic acid; In water; for 12h; Inert atmosphere; Reflux;

DOI:10.1021/ol801007m

upstream raw materials:

methanol

glyceric acid

acrylic acid methyl ester

(+/-)-calcium glycerate dihydrate

Downstream raw materials:

methyl 2,2-dimethyl-1,3-dioxolane-4-carboxylate

2,3-dihydroxy-N,N-dimethylpropionamide

methyl (4S)-2,2-dimethyl-1,3-dioxolane-4-carboxylate

methyl (R)-2,2-dimethyl-1,3-dioxolane-4-carboxylate