1,1,1-trichloro-2-fluoro-ethane

Base Information

• Chemical Name: 1,1,1-trichloro-2-fluoro-ethane
• CAS No.: 2366-36-1
• Molecular Formula: C2H2 Cl3 F
• Molecular Weight: 151.395
• Hs Code.: 2903791090
• Mol file: 2366-36-1.mol

Synonyms:1,1,1-Trichloro-2-fluoro-ethane

Chemical Property of 1,1,1-trichloro-2-fluoro-ethane

Chemical Property:

• Melting Point: -103.15°C
• Refractive Index: 1.4189 (estimate)
• Boiling Point: 94.8°Cat760mmHg
• Flash Point: 6.2°C
• PSA: 0.00000
• Density: 1.495g/cm³
• LogP: 2.32610

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,1,1-trichloro-2-fluoro-ethane

There total 3 articles about 1,1,1-trichloro-2-fluoro-ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1-Dichloroethylene (75-35-4,9002-85-1) → 1,1,2-trichloro-1-fluoroethane (811-95-0) + 1,1,1-trichlorofluoroethane (2366-36-1) + Trichloroethylene (79-01-6) + trichloroethyl acetate (84816-01-3)

Guidance literature:

With chlorine monofluoride; In 1,1,2-Trichloro-1,2,2-trifluoroethane; ethyl acetate; at 20 - 25 ℃; for 0.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

Reference yield:

1,1-Dichloroethylene (75-35-4,9002-85-1) + ethyl acetate (141-78-6) → 1,1,2-trichloro-1-fluoroethane (811-95-0) + 1,1,1-trichlorofluoroethane (2366-36-1) + Trichloroethylene (79-01-6) + trichloroethyl acetate (84816-01-3)

Guidance literature:

With chlorine monofluoride; In 1,1,2-Trichloro-1,2,2-trifluoroethane; at 20 - 25 ℃; for 0.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

Reference yield:

ethanol (64-17-5) + 1,1-Dichloroethylene (75-35-4,9002-85-1) + ethyl acetate (141-78-6) → 1,1,2-trichloro-1-fluoroethane (811-95-0) + 1,1,1-trichlorofluoroethane (2366-36-1) + Trichloroethylene (79-01-6) + chloroacetic acid ethyl ester (105-39-5)

Guidance literature:

With chlorine monofluoride; Yield given. Multistep reaction. Yields of byproduct given; 1.) Freon 113; 2.) 20 - 25 deg C, 30 min.;

upstream raw materials:

1,1-Dichloroethylene

ethanol

ethyl acetate

Downstream raw materials:

(E)-1-chloro-1,2-difluoro-2-phenylethene

(Z)-1-chloro-1,2-difluoro-2-phenylethene

Refernces