1,6-Bis(4-methylphenyl)hexane-1,6-dione

Base Information

Chemical Name:1,6-Bis(4-methylphenyl)hexane-1,6-dione
CAS No.:6280-00-8
Molecular Formula:C20H22O2
Molecular Weight:294.393
Hs Code.:
NSC Number:11032
DSSTox Substance ID:DTXSID70978464
Nikkaji Number:J1.469.538I
Wikidata:Q82963854

Synonyms:6280-00-8;1,6-bis(4-methylphenyl)hexane-1,6-dione;NSC11032;SCHEMBL9419411;DTXSID70978464;1,4-Di-(p-methyl benzoyl)-butane;NSC-11032;1,6-Bis(4-methylphenyl)-1,6-hexanedione

Suppliers and Price of 1,6-Bis(4-methylphenyl)hexane-1,6-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1,6-Bis(4-methylphenyl)hexane-1,6-dione

Chemical Property:

Vapor Pressure:7.35E-09mmHg at 25°C
Boiling Point:466°Cat760mmHg
Flash Point:173.3°C
Density:1.055g/cm³
XLogP3:4.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:7
Exact Mass:294.161979940
Heavy Atom Count:22
Complexity:322

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C(=O)CCCCC(=O)C2=CC=C(C=C2)C

Technology Process of 1,6-Bis(4-methylphenyl)hexane-1,6-dione

There total 8 articles about 1,6-Bis(4-methylphenyl)hexane-1,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 40122-37-0
1-(p-tolyl)cyclopropan-1-ol

: 6280-00-8
1,6-bis(p-methylphenyl)-1,6-hexanedione

Guidance literature:: With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver carbonate; In 2,2,2-trifluoroethanol; at 20 ℃; for 0.25h; Schlenk technique; Sealed tube; Inert atmosphere;
DOI:10.1021/acs.orglett.0c00967

Reference yield: 60.0%

: 111-50-2
Adipic acid dichloride

: 108-88-3,15644-74-3,16713-13-6
toluene

: 6280-00-8
1,6-bis(p-methylphenyl)-1,6-hexanedione

Guidance literature:: With aluminum (III) chloride; at 50 - 60 ℃; for 2h;
DOI:10.1002/jhet.1034

Reference yield: 46.0%

: 3457-48-5
1,2-di(4-methylphenyl)-1,2-ethanedione

: 917-57-7
vinyllithium

: 6280-00-8
1,6-bis(p-methylphenyl)-1,6-hexanedione

: cis-2-p-methylbenzoyl-1-(p-methylphenyl)cyclopentanol

Guidance literature:: 1,2-di(4-methylphenyl)-1,2-ethanedione; vinyllithium; In tetrahydrofuran; diethyl ether; at -78 ℃; for 1.5h;

With ammonium chloride; In diethyl ether; at -78 ℃; for 1h;
DOI:10.1002/1099-0690(200101)2001:1<93::AID-EJOC93>3.0.CO;2-X