Acetamide, 2-chloro-N-[[(2S)-4-[(3,4-dichlorophenyl)methyl]-2-morpholinyl]methyl]-

Base Information

• Chemical Name: Acetamide, 2-chloro-N-[[(2S)-4-[(3,4-dichlorophenyl)methyl]-2-morpholinyl]methyl]-
• CAS No.: 879402-30-9
• Molecular Formula: C14H17Cl3N2O2
• Molecular Weight: 351.66

Synonyms:(2S)-N-{[4-(3,4-dichlorobenzyl)morpholin-2-yl]methyl}chloroacetamide;

Chemical Property of Acetamide, 2-chloro-N-[[(2S)-4-[(3,4-dichlorophenyl)methyl]-2-morpholinyl]methyl]-

Chemical Property:

• PSA: 41.57000
• LogP: 2.87800

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Acetamide, 2-chloro-N-[[(2S)-4-[(3,4-dichlorophenyl)methyl]-2-morpholinyl]methyl]-

There total 5 articles about Acetamide, 2-chloro-N-[[(2S)-4-[(3,4-dichlorophenyl)methyl]-2-morpholinyl]methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2S)-2-aminomethyl-4-(3,4-dichlorobenzyl)morpholine (407640-11-3) + chloroacetyl chloride (79-04-9) → (2S)-N-{[4-(3,4-dichlorobenzyl)morpholin-2-yl]methyl}chloroacetamide (879402-30-9)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 2h;

Reference yield:

(2S)-2-aminomethyl-4-(3,4-dichlorobenzyl)morpholine dihydrochloride + chloroacetyl chloride (79-04-9) → (2S)-N-{[4-(3,4-dichlorobenzyl)morpholin-2-yl]methyl}chloroacetamide (879402-30-9)

Guidance literature:

With sodium hydrogencarbonate; In chloroform; water; at 0 - 30 ℃; for 3h;

Reference yield:

(2S)-2-aminomethyl-4-(3,4-dichlorobenzyl)morpholine dihydrochloride + chloroacetyl chloride (79-04-9) → (2S)-N-{[4-(3,4-dichlorobenzyl)morpholin-2-yl]methyl}chloroacetamide (879402-30-9)

Guidance literature:

With sodium hydrogencarbonate; In tert-butyl methyl ether; water; at 0 - 20 ℃; for 3.16667h;

upstream raw materials:

(2S)-2-aminomethyl-4-(3,4-dichlorobenzyl)morpholine

chloroacetyl chloride

2-{[(2R)-4-(3,4-dichlorobenzyl)morpholin-2-yl]methyl}-1H-isoindole-1,3-(2H)-dione

Downstream raw materials:

(2S)-[4-(carboxymethyl)thiazol-2-ylthio]-N-{[4-(3,4-dichlorobenzyl)morpholin-2-yl]methyl}acetamide

(2S)-[4-(carboxymethyl)thiazol-2-ylthio]-N-{[4-(3,4-dichlorobenzyl)morpholin-2-yl]methyl}acetamide hydrobromide

(2S)-N-{[4-(3,4-dichlorobenzyl)morpholin-2-yl]methyl}chloroacetamide hydrochloride

(S)-2-acetylsulfanyl-N-((4-((3,4-dichlorophenyl)methyl)morpholin-2-yl)methyl)acetamide

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