Stannane, (3-methoxypropyl)triphenyl-

Base Information

Chemical Name:Stannane, (3-methoxypropyl)triphenyl-
CAS No.:881192-37-6
Molecular Formula:C22H24OSn
Molecular Weight:423.142
Hs Code.:

Synonyms:

Suppliers and Price of Stannane, (3-methoxypropyl)triphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Stannane, (3-methoxypropyl)triphenyl-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Stannane, (3-methoxypropyl)triphenyl-

There total 2 articles about Stannane, (3-methoxypropyl)triphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 36215-07-3
1-Chloro-3-methoxypropane

: 639-58-7
triphenyltin chloride

: 881192-37-6
(3-methoxypropyl)triphenylstannane

Guidance literature:: With Mg; 1,2-dibromoethane; In tetrahydrofuran; soln. of ligand (27.63 mmol) in THF added to Mg chips activated with I2 vapor (1,2-dibromoethane activator), refluxed for 1 h, cooled to -50°C, soln. of Sn compd. (18.63 mmol) added dropwise, refluxed for 8 h; cooled to room temp., filtered, H2O added, extd. (Et2O), org. layer dried (Na2SO4), evapd., recrystd. (CHCl3/hexane), elem. anal.;
DOI:10.1002/ejic.200400877

Reference yield:

: 33304-76-6
3-(triphenylstannyl)-1-propanol

: 881192-37-6
(3-methoxypropyl)triphenylstannane

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; trimethylamine hydrochloride / dichloromethane / 2 h / 20 °C / Inert atmosphere; Schlenk technique

2: acetonitrile; methanol / 80 °C / Inert atmosphere; Schlenk technique

With trimethylamine hydrochloride; triethylamine; In methanol; dichloromethane; acetonitrile;
DOI:10.1002/ejic.202100937

Reference yield: 98.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 881192-37-6
(3-methoxypropyl)triphenylstannane

: dichloro(3-methoxypropyl)phenylstannane

Guidance literature:: In chloroform; byproducts: C6H6; stoich. mixt., chloroform soln. of HCl added to soln. of metal compd., stirred at room temp. for 2 d; evapd., recrystd. (CHCl3/hexane), elem. anal.;
DOI:10.1002/ejic.200400877