3-(Triphenylstannyl)propan-1-ol

Base Information

Chemical Name:3-(Triphenylstannyl)propan-1-ol
CAS No.:33304-76-6
Molecular Formula:C21H22 O Sn
Molecular Weight:409.115
Hs Code.:
NSC Number:179750,227362
DSSTox Substance ID:DTXSID70306783

Synonyms:33304-76-6;NSC179750;3-(Triphenylstannyl)propan-1-ol;DTXSID70306783;NSC227362;NSC-179750;NSC-227362

Suppliers and Price of 3-(Triphenylstannyl)propan-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of 3-(Triphenylstannyl)propan-1-ol

Chemical Property:

Vapor Pressure:8.29E-10mmHg at 25°C
Boiling Point:474.4°C at 760 mmHg
Flash Point:240.7°C
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:6
Exact Mass:410.069268
Heavy Atom Count:23
Complexity:279

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)[Sn](CCCO)(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of 3-(Triphenylstannyl)propan-1-ol

There total 3 articles about 3-(Triphenylstannyl)propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 892-20-6
triphenylstannane

: 107-18-6
allyl alcohol

: 33304-76-6
3-(triphenylstannyl)-1-propanol

Guidance literature:: addition of (C6H5)3SnH to CH2=CHCH2OH at 80-100 °C in presence of AlBN;;

Reference yield: 85.0%

: 892-20-6
triphenylstannane

: 107-18-6
allyl alcohol

: 799278-88-9
(C₆H₅)3SnCH(CH₃)CH₂OH

: 33304-76-6
3-(triphenylstannyl)-1-propanol

Guidance literature:: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In tetrahydrofuran; under exclusion of moisture and air; Ph3SnH, THF and Pd complex (0.01 equiv.) at -78°C added to allylic alcohol (2 equiv.); warmed to room temp. for 16 h under stirring; volatiles removed; sepd. by chromy. (SiO2, gradient petroleum ether-ethyle acetate from 5:1 to 1:1, ethyl acetate); elem. anal.;
DOI:10.1016/j.jorganchem.2004.06.065