1,5,9-Triazacyclododecane, 1,5-bis[(4-methoxyphenyl)sulfonyl]-3-methylene-9-(phenylmethyl)-

Base Information

Chemical Name:1,5,9-Triazacyclododecane, 1,5-bis[(4-methoxyphenyl)sulfonyl]-3-methylene-9-(phenylmethyl)-
CAS No.:881693-71-6
Molecular Formula:C31H39N3O6S2
Molecular Weight:613.799
Hs Code.:

Synonyms:

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Chemical Property of 1,5,9-Triazacyclododecane, 1,5-bis[(4-methoxyphenyl)sulfonyl]-3-methylene-9-(phenylmethyl)-

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Technology Process of 1,5,9-Triazacyclododecane, 1,5-bis[(4-methoxyphenyl)sulfonyl]-3-methylene-9-(phenylmethyl)-

There total 5 articles about 1,5,9-Triazacyclododecane, 1,5-bis[(4-methoxyphenyl)sulfonyl]-3-methylene-9-(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: N,N'-bis(p-methoxybenzenesulfonyl)bis(3-aminopropyl)benzylamine hydrochloride

: 1871-57-4
2-chloromethyl-3-chloroprop-1-ene

: 881693-71-6
KKD₀₂₃

Guidance literature:: N,N'-bis(p-methoxybenzenesulfonyl)bis(3-aminopropyl)benzylamine hydrochloride; With sodium hydride; In N,N-dimethyl-formamide; at 75 ℃;

2-chloromethyl-3-chloroprop-1-ene; In N,N-dimethyl-formamide; at 60 ℃; for 48h;
DOI:10.1021/jm0582524

Reference yield:

: 782-87-6
N-benzylbis(2-cyanoethyl)amine

: 881693-71-6
KKD₀₂₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen; sodium hydroxide / ethanol / Inert atmosphere

2.1: sodium hydroxide / dichloromethane; water / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide / Inert atmosphere

3.2: 85 °C / Inert atmosphere

With hydrogen; sodium hydride; sodium hydroxide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm2002603

Reference yield:

: 111-94-4
3,3'-Iminodipropionitrile

: 881693-71-6
KKD₀₂₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium carbonate; sodium iodide / acetonitrile / Inert atmosphere

2.1: hydrogen; sodium hydroxide / ethanol / Inert atmosphere

3.1: sodium hydroxide / dichloromethane; water / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide / Inert atmosphere

4.2: 85 °C / Inert atmosphere

With hydrogen; sodium hydride; sodium carbonate; sodium iodide; sodium hydroxide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm2002603