Thymidine, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-, 3'-[hydrogen (4-chlorobenzoyl)phosphonate], compd. with N,N-diethylethanamine (1:1)

Base Information

Chemical Name:Thymidine, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-, 3'-[hydrogen (4-chlorobenzoyl)phosphonate], compd. with N,N-diethylethanamine (1:1)
CAS No.:89849-86-5
Molecular Formula:C38H36ClN2O10P.C6H15N
Molecular Weight:848.33
Hs Code.:

Thymidine, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-, 3'-[hydrogen
(4-chlorobenzoyl)phosphonate], compd. with N,N-diethylethanamine
(1:1)

Synonyms:

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Chemical Property of Thymidine, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-, 3'-[hydrogen (4-chlorobenzoyl)phosphonate], compd. with N,N-diethylethanamine (1:1)

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Technology Process of Thymidine, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-, 3'-[hydrogen (4-chlorobenzoyl)phosphonate], compd. with N,N-diethylethanamine (1:1)

There total 2 articles about Thymidine, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-, 3'-[hydrogen (4-chlorobenzoyl)phosphonate], compd. with N,N-diethylethanamine (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66190-99-6
C₁₃H₂₂ClO₄PSi₂

: 89849-86-5
triethylammonium 5'-O-(dimethoxytrityl)thymidine (p-chlorobenzoyl)phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂O / methanol / 0.08 h

2: 976 mg / mesitylene-1,3-disulfonyl chloride (MDS), pyridine / Ambient temperature

With pyridine; mesitylene-1,3-disulfonyl chloride; water; In methanol;
DOI:10.1021/jo00186a012

Reference yield:

: 66191-03-5
p-Chlorobenzoylphosphonic acid

: 15715-58-9
triethylamine carbonate

: 40615-39-2
5'-O-(4-4'-dimethoxytrityl)thymidine

: 89849-86-5
triethylammonium 5'-O-(dimethoxytrityl)thymidine (p-chlorobenzoyl)phosphonate

Guidance literature:: With pyridine; mesitylene-1,3-disulfonyl chloride; Ambient temperature;
DOI:10.1021/jo00186a012

Reference yield: 66.0%

: 21090-30-2
3'-O-acetylthymidine

: 89849-86-5
triethylammonium 5'-O-(dimethoxytrityl)thymidine (p-chlorobenzoyl)phosphonate

: 89849-89-8
C₅₀H₅₀ClN₄O₁₅P

Guidance literature:: With mesitylen-1,3-disulfonyl chloride; 3-nitro-1,2,4-triazole; In pyridine; for 1h; Ambient temperature;
DOI:10.1021/jo00186a012