Benzene, 2-azido-5-methoxy-1,3-dinitro-

Base Information

Chemical Name:Benzene, 2-azido-5-methoxy-1,3-dinitro-
CAS No.:90403-59-1
Molecular Formula:C7H5N5O5
Molecular Weight:239.147
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, 2-azido-5-methoxy-1,3-dinitro-

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Technology Process of Benzene, 2-azido-5-methoxy-1,3-dinitro-

There total 5 articles about Benzene, 2-azido-5-methoxy-1,3-dinitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 5350-56-1
4-amino-1-methoxy-3,5-dinitrobenzene

: 90403-59-1
4-methoxy-2,6-dinitrophenyl azide

Guidance literature:: With sodium azide; sulfuric acid; sodium nitrite; 1.) 40 degC, 2.) water, acetic acid, 60 degC;

Reference yield:

: 104-94-9
4-methoxy-aniline

: 90403-59-1
4-methoxy-2,6-dinitrophenyl azide

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid / 0.25 h / Heating

2: 60percent nitric acid, conc. sulfuric acid / 1.) 0 deg C, 10 min, 2.) RT, 30 min

3: 60percent nitric acid, conc. sulfuric acid / 1.) 0 deg C, 10 min, 2.) RT, 30 min

4: conc. sulfuric acid / 0.25 h / 100 °C

5: 1.) aq. HCl, NaNO₂, 2.) aq. NaN₃, sodium acetate / 1.) 0 deg C, 15 min

With hydrogenchloride; sodium azide; sulfuric acid; nitric acid; sodium acetate; sodium nitrite; In acetic acid;
DOI:10.1021/jm00010a023

Reference yield:

: 119-81-3
4-methoxy-2-nitroacetanilide

: 90403-59-1
4-methoxy-2,6-dinitrophenyl azide

Guidance literature:: Multi-step reaction with 3 steps

1: 60percent nitric acid, conc. sulfuric acid / 1.) 0 deg C, 10 min, 2.) RT, 30 min

2: conc. sulfuric acid / 0.25 h / 100 °C

3: 1.) aq. HCl, NaNO₂, 2.) aq. NaN₃, sodium acetate / 1.) 0 deg C, 15 min

With hydrogenchloride; sodium azide; sulfuric acid; nitric acid; sodium acetate; sodium nitrite;
DOI:10.1021/jm00010a023