Ethanamine;nitric acid

Base Information

• Chemical Name: Ethanamine;nitric acid
• CAS No.: 22113-86-6
• Molecular Formula: C2H8N2O3
• Molecular Weight: 108.097
• Hs Code.: 2923900090
• European Community (EC) Number: 690-858-8
• DSSTox Substance ID: DTXSID0047901
• Wikipedia: Ethylammonium_nitrate
• ChEMBL ID: CHEMBL3186052
• Mol file: 22113-86-6.mol

Synonyms:ethylammonium;ethylammonium nitrate

Chemical Property of Ethanamine;nitric acid

Chemical Property:

• Vapor Pressure: 49.8mmHg at 25°C
• Melting Point: 8 °C
• Boiling Point: 83 ºC at 760 mmHg
• Flash Point: °C
• PSA: 27.64000
• Density: g/cm³
• LogP: -0.75180
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 0
• Exact Mass: 108.05349212
• Heavy Atom Count: 7
• Complexity: 27.5

Purity/Quality:

99%, ^*data from raw suppliers

ETHYLAMMONIUM NITRATE 97.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCN.[N+](=O)(O)[O-]

Technology Process of Ethanamine;nitric acid

There total 1 articles about Ethanamine;nitric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

ethylamine (75-04-7,85404-22-4) → ethylammonium nitrate (22113-86-6)

Guidance literature:

With nitric acid; In water; at 10 ℃; pH=7.3;

DOI:10.1016/j.bmcl.2011.02.039

Reference yield: 97.0%

ethylammonium nitrate (22113-86-6) + 4-dimethylamino-benzaldehyde (100-10-7) → 4-[(ethylimino)methyl]-N,N-dimethylbenzeneamine (59488-00-5)

Guidance literature:

pH=6;

DOI:10.1002/poc.1501

Reference yield: 86.0%

ethylammonium nitrate (22113-86-6) + anthranilic acid amide (28144-70-9,88-68-6) + orthoformic acid triethyl ester (122-51-0) → 4-Hydroxyquinazoline (491-36-1) + 3-ethyl-3H-quinazoline-4-one (3476-65-1)

Guidance literature:

at 45 - 46 ℃; for 0.333333h; Ionic liquid; Sonication; neat (no solvent);

DOI:10.1002/ejoc.201100128

upstream raw materials:

ethylamine

Downstream raw materials:

ethyl guanidine

acetaldehyde

ethyl nitrite

ethanol

Refernces

• 1、 Yasui, Kazutoshi,Uegaki, Masamichi,Shiraki, Kentaro,Ishimizu, Takeshi. "Enhanced solubilization of membrane proteins by alkylamines and polyamines". . p. 486 - 493. Retrieved 2010.
• 2、 Dai, Caili,Du, Mingyong,Liu, Yifei,Wang, Shilu,Zhao, Jianhui,Chen, Ang,Peng, Dongxu,Zhao, Mingwei. "Aggregation behavior of long-chain piperidinium ionic liquids in ethylammonium nitrate". . p. 20157 - 20169. Retrieved 2014.
• 3、 Tian, Tongtong,Hu, Qiongzheng,Wang, Yi,Gao, Yanan,Yu, Li. "Reversible Photoresponsive Molecular Alignment of Liquid Crystals at Fluid Interfaces with Persistent Stability". . p. 6340 - 6344. Retrieved 2016.
• 4、 Zhao, Mingwei,Gao, Yanan,Zheng, Liqiang. "Liquid crystalline phases of the amphiphilic ionic liquid n -hexadecyl- n -methylpyrrolidinium bromide formed in the ionic liquid ethylammonium nitrate and in water". . p. 11382 - 11389. Retrieved 2010.
• 5、 Zhou, Fengling,McDonnell-Worth, Ciaran,Li, Haitao,Li, Jiaye,Spiccia, Leone,MacFarlane, Douglas R.. "Enhanced photo-electrochemical water oxidation on MnOx in buffered organic/inorganic electrolytes". . p. 16642 - 16652. Retrieved 2015.
• 6、 Bravo, María V.,Fernández, José L.,Adam, Claudia G.,Della Rosa, Claudia D.. "Understanding the Role of Protic Ionic Liquids (PILs) in Reactive Systems: Rational Selection of PILs for the Design of Green Synthesis Strategies for Allylic Amines and β-Amino Esters". . p. 919 - 926. Retrieved 2019/07/31.