1,2-Dibromo-4-iodobenzene

Base Information

Chemical Name:1,2-Dibromo-4-iodobenzene
CAS No.:909072-74-8
Molecular Formula:C6H3Br2I
Molecular Weight:361.802
Hs Code.:2903998090
European Community (EC) Number:834-536-9
Nikkaji Number:J2.917.369I
Mol file:909072-74-8.mol

Synonyms:1,2-DIBROMO-4-IODOBENZENE;909072-74-8;3,4-Dibromoiodobenzene;MFCD09753707;Benzene, 1,2-dibromo-4-iodo-;SCHEMBL9575829;SY234718;CS-0192406;D5493;T73057

Suppliers and Price of 1,2-Dibromo-4-iodobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1,2-Dibromo-4-iodobenzene
1g
$ 100.00

TCI Chemical
1,2-Dibromo-4-iodobenzene
5G
$ 241.00

TCI Chemical
1,2-Dibromo-4-iodobenzene
1G
$ 80.00

Apolloscientific
1,2-Dibromo-4-iodobenzene 98%
1g
$ 56.00

Apolloscientific
1,2-Dibromo-4-iodobenzene 98%
5g
$ 134.00

Apolloscientific
1,2-Dibromo-4-iodobenzene 98%
25g
$ 493.00

AOBChem
1,2-Dibromo-4-iodobenzene 97%
10g
$ 252.00

Alichem
3,4-Dibromoiodobenzene
1g
$ 1549.60

Alichem
3,4-Dibromoiodobenzene
500mg
$ 790.55

Alichem
3,4-Dibromoiodobenzene
250mg
$ 489.60

Total 17 raw suppliers

Chemical Property of 1,2-Dibromo-4-iodobenzene

Chemical Property:

Melting Point:57-59 °C(Solv: hexane (110-54-3))
Boiling Point:306.0±27.0 °C(Predicted)
PSA：0.00000
Density:2.514±0.06 g/cm3(Predicted)
LogP:3.81620
Storage Temp.:-20°C Freezer
Solubility.:Chloroform (Slightly), Methanol (Slightly)
XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:361.76257
Heavy Atom Count:9
Complexity:97.1

Purity/Quality:

97% ^*data from raw suppliers

1,2-Dibromo-4-iodobenzene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C=C1I)Br)Br

Technology Process of 1,2-Dibromo-4-iodobenzene

There total 3 articles about 1,2-Dibromo-4-iodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 3,4-dibromobenzenediazonium tetrafluoroborate

: 909072-74-8
1,2-dibromo-4-iodobenzene

Guidance literature:: With potassium iodide; In water; acetone; at 25 ℃; for 0.5h;
DOI:10.1002/ejoc.201001217

Reference yield:

: 615-55-4
3,4-dibromoaniline

: 909072-74-8
1,2-dibromo-4-iodobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: tetrafluoroboric acid; sodium nitrite / water / 0.5 h / 0 °C

2: potassium iodide / water; acetone / 0.5 h / 25 °C

With tetrafluoroboric acid; potassium iodide; sodium nitrite; In water; acetone; 2: Sandmeyer iodination;
DOI:10.1002/ejoc.201001217

Reference yield:

: 591-19-5
m-Bromoaniline

: 909072-74-8
1,2-dibromo-4-iodobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: tetra-N-butylammonium tribromide / dichloromethane / 0.5 h / 25 °C

2: tetrafluoroboric acid; sodium nitrite / water / 0.5 h / 0 °C

3: potassium iodide / water; acetone / 0.5 h / 25 °C

With tetrafluoroboric acid; tetra-N-butylammonium tribromide; potassium iodide; sodium nitrite; In dichloromethane; water; acetone; 3: Sandmeyer iodination;
DOI:10.1002/ejoc.201001217