p-Ethoxyphenylarsonic acid

Base Information

• Chemical Name: p-Ethoxyphenylarsonic acid
• CAS No.: 6269-93-8
• Molecular Formula: C8H11AsO4
• Molecular Weight: 246.0921
• Mol file: 6269-93-8.mol

Synonyms:R DO2;p-Ethoxybenzenearsonic acid;4-ethoxyphenylarsonic acid;Benzenearsonic acid,p-ethoxy;

Chemical Property of p-Ethoxyphenylarsonic acid

Chemical Property:

• Vapor Pressure: 2.97E-09mmHg at 25°C
• Boiling Point: 459.9°Cat760mmHg
• Flash Point: 187.6°C
• PSA: 66.76000
• Density: g/cm³
• LogP: -0.35370

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of p-Ethoxyphenylarsonic acid

There total 1 articles about p-Ethoxyphenylarsonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethanol (64-17-5) + 4-fluoroaniline (371-40-4) → 4-ethoxyphenylarsonic acid (6269-93-8)

Guidance literature:

4-fluoroaniline; With sulfuric acid; arsenic trichloride; sodium nitrite; In ethanol; water; at 0 - 5 ℃;

ethanol; copper(I) bromide; In water; at 60 ℃; for 6h; Further stages.;

DOI:10.1016/j.jorganchem.2008.04.033

Reference yield: 61.3%

1.3-propanedithiol (109-80-8) + 4-ethoxyphenylarsonic acid (6269-93-8) → 2-(4-ethoxyphenyl)-1,3,2-dithiaarsinane

Guidance literature:

4-ethoxyphenylarsonic acid; With ammonium 2-sulfanylacetate; In ethanol; at 55 ℃; for 1h;

1.3-propanedithiol; In ethanol; for 0.5h;

DOI:10.1021/acs.inorgchem.6b01175

Reference yield: 47.0%

4-ethoxyphenylarsonic acid (6269-93-8) + ethane-1,2-dithiol (540-63-6) → 2-(4-ethoxyphenyl)-1,3,2-dithiaarsolane

Guidance literature:

4-ethoxyphenylarsonic acid; With ammonium 2-sulfanylacetate; In ethanol; at 55 ℃; for 1h;

ethane-1,2-dithiol; In ethanol; for 0.5h;

DOI:10.1021/acs.inorgchem.6b01175

upstream raw materials:

ethanol

4-fluoroaniline

Refernces