2-(4-Bromo-2-methylphenyl)-1,3-dioxolane

Base Information

Chemical Name:2-(4-Bromo-2-methylphenyl)-1,3-dioxolane
CAS No.:91587-27-8
Molecular Formula:C10H11BrO2
Molecular Weight:243.1
Hs Code.:
DSSTox Substance ID:DTXSID20693135
Wikidata:Q82622153

Synonyms:2-(4-bromo-2-methylphenyl)-1,3-dioxolane;91587-27-8;1,3-Dioxolane, 2-(4-bromo-2-methylphenyl)-;1,3-Dioxolane,2-(4-bromo-2-methylphenyl)-;SCHEMBL3830652;DTXSID20693135;ZJJDARIPEHETAJ-UHFFFAOYSA-N;MFCD19441484;AKOS015995063;CS-0193431;E91870;EN300-8155790;J-503938

Suppliers and Price of 2-(4-Bromo-2-methylphenyl)-1,3-dioxolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2-(4-Bromo-2-methylphenyl)-1,3-dioxolane

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:241.99424
Heavy Atom Count:13
Complexity:168

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=CC(=C1)Br)C2OCCO2

Technology Process of 2-(4-Bromo-2-methylphenyl)-1,3-dioxolane

There total 3 articles about 2-(4-Bromo-2-methylphenyl)-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68837-59-2
4-bromo-2-methylbenzoic acid

: 91587-27-8
2-(4-bromo-2-methylphenyl)-1,3-dioxolane

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / BH₃*THF / tetrahydrofuran / 1 h / 0 - 20 °C

2: PCC / CH₂Cl₂ / 2.5 h

3: p-TsOH*H₂O / benzene / 17 h / Heating

With borane-THF; toluene-4-sulfonic acid; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1021/jm00377a022

Reference yield:

: 17100-58-2
4-bromo-2-methylbenzyl alcohol

: 91587-27-8
2-(4-bromo-2-methylphenyl)-1,3-dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: PCC / CH₂Cl₂ / 2.5 h

2: p-TsOH*H₂O / benzene / 17 h / Heating

With toluene-4-sulfonic acid; pyridinium chlorochromate; In dichloromethane; benzene;
DOI:10.1021/jm00377a022