Benzoic acid, 2-(2-bromoethoxy)-, methyl ester

Base Information

Chemical Name:Benzoic acid, 2-(2-bromoethoxy)-, methyl ester
CAS No.:91687-70-6
Molecular Formula:C10H11BrO3
Molecular Weight:259.1
Hs Code.:

Synonyms:(β-Brom-aethylaether)-salicylsaeure-methylester;2-(β-Brom-aethoxy)-benzoesaeuremethylester;methyl 2-(2-bromoethoxy)benzoate;2-[2-Bromoethoxy]benzoic acid, methyl ester;2-(2-bromo-ethoxy)-benzoic acid methyl ester;2-(2-Brom-aethoxy)-benzoesaeure-methylester;

Suppliers and Price of Benzoic acid, 2-(2-bromoethoxy)-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AK Scientific
Methyl2-(2-bromoethoxy)benzoate
500mg
$ 364.00

Total 3 raw suppliers

Chemical Property of Benzoic acid, 2-(2-bromoethoxy)-, methyl ester

Chemical Property:

Boiling Point:186 - 188 °C (20 mmHg)
PSA：35.53000
LogP:2.24690

Purity/Quality:: Methyl2-(2-bromoethoxy)benzoate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 2-(2-bromoethoxy)-, methyl ester

There total 4 articles about Benzoic acid, 2-(2-bromoethoxy)-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 106-93-4
ethylene dibromide

: 119-36-8,8024-54-2
methyl salicylate

: 91687-70-6
2-(2-bromoethoxy)benzoic acid methyl ester

Guidance literature:: With potassium carbonate; In acetonitrile; for 6h; Reflux;

Reference yield:

: (+-)-5-[[2H-3,4,5,6-Tetrahydropyran-2-yl]oxymethyl]phenyl-1,3-bis[oxyacetic acid]

: 106-93-4
ethylene dibromide

: 119-36-8,8024-54-2
methyl salicylate

: 91687-70-6
2-(2-bromoethoxy)benzoic acid methyl ester

Guidance literature:: In 2-Methylpentane;

Reference yield:

: 69-72-7,25496-36-0,8052-31-1
salicylic acid

: 91687-70-6
2-(2-bromoethoxy)benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / 6 h / Reflux

2: potassium carbonate / dimethyl sulfoxide / 3.5 h / 20 °C

With sulfuric acid; potassium carbonate; In dimethyl sulfoxide;
DOI:10.2174/1570180811666140627004607