acofriose

Base Information

• Chemical Name: acofriose
• CAS No.: 4598-54-3
• Molecular Formula: C₇H₁₄O₅
• Molecular Weight: 178.185
• Mol file: 4598-54-3.mol

Synonyms:4-Hydroxy-3-(8-phenyloctyl)chromen-2-one;2H-1-Benzopyran-2-one,4-hydroxy-3-(8-phenyloctyl)-;3-(omega-Phenyloctyl)-4-hydroxycoumarin;

Chemical Property of acofriose

Chemical Property:

• Vapor Pressure: 1.4E-07mmHg at 25°C
• Boiling Point: 386.8°Cat760mmHg
• Flash Point: 159.7°C
• PSA: 0.00000
• Density: 1.256g/cm³
• LogP: 0.00000

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of acofriose

There total 45 articles about acofriose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

C31H46O10 (1279102-01-0) → 6-deoxy-3-O-methyl-D-allose (523-74-0,642-33-1,4060-08-6,4481-08-7,4598-54-3,5158-56-5,7045-53-6,14064-39-2,17212-18-9,18546-08-2,18546-09-3,18546-11-7,25374-97-4,51795-06-3,91741-22-9,117857-64-4,149655-76-5,5675-98-9,18546-13-9)

Guidance literature:

With sulfuric acid; water; In 1,4-dioxane; for 2h;

DOI:10.1039/c0ob00677g

Reference yield:

glaucogenin C 3-O-b-D-glucopyranosyl-(14)-b-D-cymaropyranosyl-(14)-b-D-digitoxopyranosyl-(14)-b-D-thevetopyranoside → D-digitxose (527-52-6) + D-symarose (13089-76-4) + 6-deoxy-3-O-methyl-D-allose (523-74-0,642-33-1,4060-08-6,4481-08-7,4598-54-3,5158-56-5,7045-53-6,14064-39-2,17212-18-9,18546-08-2,18546-09-3,18546-11-7,25374-97-4,51795-06-3,91741-22-9,117857-64-4,149655-76-5,5675-98-9,18546-13-9) + D-glucose (50-99-7)

Guidance literature:

With hydrogenchloride; In methanol; water; at 70 ℃; for 0.25h;

DOI:10.1016/j.cclet.2017.05.017

Reference yield:

12-O-cinnamoyl-20-O-nicotinoylsarcostin 3-O-β-D-glucopyranosyl-(1→4)-β-D-thevetopyranosyl-(1→4)-β-D-oleandropyranosyl-(1→4)-β-D-cymaropyranoside → D-symarose (13089-76-4) + D-oleandrose (13089-77-5) + 6-deoxy-3-O-methyl-D-allose (523-74-0,642-33-1,4060-08-6,4481-08-7,4598-54-3,5158-56-5,7045-53-6,14064-39-2,17212-18-9,18546-08-2,18546-09-3,18546-11-7,25374-97-4,51795-06-3,91741-22-9,117857-64-4,149655-76-5,5675-98-9,18546-13-9) + D-glucose (50-99-7)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; water; at 80 ℃; for 3h;

DOI:10.1080/14786419.2020.1729153

upstream raw materials:

6-deoxy-1,2-O-isopropylidene-3-O-methyl-α-D-glucofuranose

C₃₂H₄₄O₁₁

glaucogenin-C 3-O-β-D-thevetopyranoside

5,6-anhydro-1,2-O-isopropylidene-α-D-glucofuranose

Downstream raw materials:

O³-methyl-D-arabino-6-deoxy-[2]hexosulose-bis-phenylhydrazone

O³-methyl-D-ribo-6-deoxy-[2]hexosulose-bis-phenylhydrazone

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