Technology Process of 2,4-Pentadienoic acid,
3-(dimethoxymethyl)-5-(4-methoxy-2,6,6-trimethyl-1-cyclohexen-1-yl)-,
methyl ester, (E,E)-
There total 3 articles about 2,4-Pentadienoic acid,
3-(dimethoxymethyl)-5-(4-methoxy-2,6,6-trimethyl-1-cyclohexen-1-yl)-,
methyl ester, (E,E)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 59 percent / piperidine / methanol / 27 h / Heating
2: 69 percent / 15 percent n-buthyl lithium / 1,2-dimethoxy-ethane; hexane / 3 h / Heating
With
piperidine; n-butyllithium;
In
methanol; 1,2-dimethoxyethane; hexane;
DOI:10.1248/cpb.32.1709
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) ozone gas, 2.) zinc dust, 50 percent acetic acid / 1.) methanol, -20 degC, 3 h, 2.) methanol, room temperature, 1 h
2: 59 percent / piperidine / methanol / 27 h / Heating
3: 69 percent / 15 percent n-buthyl lithium / 1,2-dimethoxy-ethane; hexane / 3 h / Heating
With
piperidine; n-butyllithium; ozone; acetic acid; zinc;
In
methanol; 1,2-dimethoxyethane; hexane;
DOI:10.1248/cpb.32.1709
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 59 percent / piperidine / methanol / 27 h / Heating
2: 69 percent / 15 percent n-buthyl lithium / 1,2-dimethoxy-ethane; hexane / 3 h / Heating
With
piperidine; n-butyllithium;
In
methanol; 1,2-dimethoxyethane; hexane;
DOI:10.1248/cpb.32.1709
