4-(Cyclohex-1-en-1-yl)-n,n-dimethylaniline

Base Information

Chemical Name:4-(Cyclohex-1-en-1-yl)-n,n-dimethylaniline
CAS No.:13314-74-4
Molecular Formula:C14H19N
Molecular Weight:201.312
Hs Code.:
NSC Number:140102
DSSTox Substance ID:DTXSID30300944
Nikkaji Number:J2.884.933H
Wikidata:Q82044396

Synonyms:13314-74-4;4-(cyclohex-1-en-1-yl)-n,n-dimethylaniline;NSC140102;DTXSID30300944;NSC-140102

Suppliers and Price of 4-(Cyclohex-1-en-1-yl)-n,n-dimethylaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 4-(Cyclohex-1-en-1-yl)-n,n-dimethylaniline

Chemical Property:

Vapor Pressure:0.000428mmHg at 25°C
Boiling Point:315.8°Cat760mmHg
Flash Point:128.6°C
Density:1.006g/cm³
XLogP3:4.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:201.151749610
Heavy Atom Count:15
Complexity:222

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)C1=CC=C(C=C1)C2=CCCCC2

Technology Process of 4-(Cyclohex-1-en-1-yl)-n,n-dimethylaniline

There total 13 articles about 4-(Cyclohex-1-en-1-yl)-n,n-dimethylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 930-66-5
1-chlorocyclohexene

: 7353-91-5
4-dimethylaminophenylmagnesium bromide

: 13314-74-4
N,N-dimethyl-2',3',4',5'-tetrahydro-[1,1'-biphenyl]-4-amine

Guidance literature:: With C₃₂H₂₆ClN₂NiP; In tetrahydrofuran; at 30 ℃; for 12h; Schlenk technique; Inert atmosphere;
DOI:10.1055/s-0033-1339653

Reference yield: 85.0%

: 7570-92-5
cyclohexyl phenyl sulphide

: 7353-91-5
4-dimethylaminophenylmagnesium bromide

: 13314-74-4
N,N-dimethyl-2',3',4',5'-tetrahydro-[1,1'-biphenyl]-4-amine

Guidance literature:: 4-dimethylaminophenylmagnesium bromide; With bis(1,5-cyclooctadiene)nickel⁽⁰⁾; 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride; In tetrahydrofuran; at 0 ℃; for 0.166667h;

cyclohexyl phenyl sulphide; In tetrahydrofuran; at 0 - 60 ℃; for 3.16667h;
DOI:10.1021/ja104155f

Reference yield: 82.0%

: 22718-22-5
cyclohex-1-en-1-yl dimethylcarbamate

: 7353-91-5
4-dimethylaminophenylmagnesium bromide

: 13314-74-4
N,N-dimethyl-2',3',4',5'-tetrahydro-[1,1'-biphenyl]-4-amine

Guidance literature:: With N,N'-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene hydrochloride; palladium diacetate; In tetrahydrofuran; at 50 ℃; for 3h; Schlenk technique; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.orglett.0c01127