diethyl (3-oxocyclohexyl)propanedioate

Base Information

Chemical Name:diethyl (3-oxocyclohexyl)propanedioate
CAS No.:22274-75-5
Molecular Formula:C13H20 O5
Molecular Weight:256.299
Hs Code.:
Mol file:22274-75-5.mol

Synonyms:Cyclohexanemalonicacid, 3-oxo-, diethyl ester (6CI,8CI); Propanedioic acid, (3-oxocyclohexyl)-,diethyl ester (9CI); Diethyl (3-oxocyclohexyl)malonate; NSC 246180

Suppliers and Price of diethyl (3-oxocyclohexyl)propanedioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of diethyl (3-oxocyclohexyl)propanedioate

Chemical Property:

Vapor Pressure:0.000101mmHg at 25°C
Boiling Point:338°Cat760mmHg
Flash Point:146°C
Density:1.123g/cm³

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of diethyl (3-oxocyclohexyl)propanedioate

There total 12 articles about diethyl (3-oxocyclohexyl)propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 930-68-7
cyclohexenone

: 105-53-3
diethyl malonate

: 22274-75-5
1,3-diethyl 2-(3-oxocyclohexyl)propanedioate

Guidance literature:: With hydrotalcite; at 80 ℃; for 6h;

Reference yield: 92.0%

: 930-68-7
cyclohexenone

: 685-87-0
Diethyl 2-bromomalonate

: 22274-75-5
1,3-diethyl 2-(3-oxocyclohexyl)propanedioate

Guidance literature:: With indium; chloro-trimethyl-silane; In tetrahydrofuran; at 20 ℃; for 0.5h; Further Variations:; Reagents; Solvents; Product distribution;
DOI:10.1021/jo026600t

Reference yield: 90.0%

: ((Si(CH₃)3O)C(CH₂)3CHCH)Fe(CO)2NO

: 996-82-7
sodium diethylmalonate

: 22274-75-5
1,3-diethyl 2-(3-oxocyclohexyl)propanedioate

Guidance literature:: In tetrahydrofuran; Stirring of mixt. at room temp. for 15 h.; Extg. (ether), washing of ext. (aq. HCL, H2O), drying (Na2SO4), evapn., chromy. (hexane-ethyl acetate), elem. anal.;
DOI:10.1246/bcsj.64.2965