Butanedioic acid, 2,3-bis(benzoyloxy)-, (2R,3R)-(6R)-compd. with 6-cyclopentyl-6-[2-(2,6-diethyl-4-pyridinyl)ethyl]-5,6-dihydro-4-hydroxy-2 H-pyran-2-one (1:1)

Base Information

Chemical Name:Butanedioic acid, 2,3-bis(benzoyloxy)-, (2R,3R)-(6R)-compd. with 6-cyclopentyl-6-[2-(2,6-diethyl-4-pyridinyl)ethyl]-5,6-dihydro-4-hydroxy-2 H-pyran-2-one (1:1)
CAS No.:927889-50-7
Molecular Formula:C21H29NO3.C18H14O8
Molecular Weight:701.771
Hs Code.:

Butanedioic acid, 2,3-bis(benzoyloxy)-, (2R,3R)-(6R)-compd. with
6-cyclopentyl-6-[2-(2,6-diethyl-4-pyridinyl)ethyl]-5,6-dihydro-4-hydroxy-2
H-pyran-2-one (1:1)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Butanedioic acid, 2,3-bis(benzoyloxy)-, (2R,3R)-(6R)-compd. with 6-cyclopentyl-6-[2-(2,6-diethyl-4-pyridinyl)ethyl]-5,6-dihydro-4-hydroxy-2 H-pyran-2-one (1:1)

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Technology Process of Butanedioic acid, 2,3-bis(benzoyloxy)-, (2R,3R)-(6R)-compd. with 6-cyclopentyl-6-[2-(2,6-diethyl-4-pyridinyl)ethyl]-5,6-dihydro-4-hydroxy-2 H-pyran-2-one (1:1)

There total 1 articles about Butanedioic acid, 2,3-bis(benzoyloxy)-, (2R,3R)-(6R)-compd. with 6-cyclopentyl-6-[2-(2,6-diethyl-4-pyridinyl)ethyl]-5,6-dihydro-4-hydroxy-2 H-pyran-2-one (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 927889-49-4
(R)-6-cyclopentyl-6-(2-(2,6-diethylpyridin-4-yl)ethyl)-dihydro-2H-pyran-2,4(3H)-dione

: 2743-38-6
O,O'-dibenzoyl-L-tartaric acid

: 927889-50-7
dibenzoyl-L-tartaric acid salt of (R)-6-cyclopentyl-6-(2,6-diethylpyridin-4-yl)ethyl-4-hydroxy-5,6-dihydropyran-2-one

Guidance literature:: In dichloromethane; tert-butyl methyl ether; at 20 - 25 ℃; for 8.16667h; Heating / reflux;

Reference yield: 67.0%

: 55293-96-4
5,7-dimethyl-[1,2,4]triazolo[1,5-a]pyrimidine-2-carbaldehyde

: 927889-50-7
dibenzoyl-L-tartaric acid salt of (R)-6-cyclopentyl-6-(2,6-diethylpyridin-4-yl)ethyl-4-hydroxy-5,6-dihydropyran-2-one

: 877130-28-4
filibuvir

Guidance literature:: 5,7-dimethyl-[1,2,4]triazolo[1,5-a]pyrimidine-2-carbaldehyde; dibenzoyl-L-tartaric acid salt of (R)-6-cyclopentyl-6-(2,6-diethylpyridin-4-yl)ethyl-4-hydroxy-5,6-dihydropyran-2-one; With borane pyridine; In tetrahydrofuran; methanol; at 20 ℃; for 3.25h;

With water; In tetrahydrofuran; methanol; dichloromethane;

With triethanolamine; In tetrahydrofuran; methanol; dichloromethane;