9-Dichloromethylenefluorene

Base Information

Chemical Name:9-Dichloromethylenefluorene
CAS No.:835-17-6
Molecular Formula:C14H8Cl2
Molecular Weight:247.124
Hs Code.:2903999090
NSC Number:126425
DSSTox Substance ID:DTXSID80298842
Nikkaji Number:J102.874J
Wikidata:Q82040918
Mol file:835-17-6.mol

Synonyms:9-Dichloromethylenefluorene;835-17-6;Fluorene, 9-(dichloromethylene)-;9H-Fluorene, 9-(dichloromethylene)-;NSC126425;9-(dichloro-methylene)-fluorene;DTXSID80298842;OAHWJMYLGMZQPX-UHFFFAOYSA-N;9-(Dichloromethylene)-9H-fluorene #;AKOS015906239;NSC-126425

Suppliers and Price of 9-Dichloromethylenefluorene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 9-Dichloromethylenefluorene

Chemical Property:

Vapor Pressure:6.5E-05mmHg at 25°C
Boiling Point:355.2°Cat760mmHg
Flash Point:154.4°C
PSA：0.00000
Density:1.373g/cm³
LogP:4.86150
XLogP3:4.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:246.0003056
Heavy Atom Count:16
Complexity:280

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C3=CC=CC=C3C2=C(Cl)Cl

Technology Process of 9-Dichloromethylenefluorene

There total 2 articles about 9-Dichloromethylenefluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 56-23-5
tetrachloromethane

: 13629-22-6
fluoren-9-ylidene-hydrazine

: 486-25-9,952573-42-1
9-fluorenone

: 746-47-4
tetrabenzo[5.5]fulvalene

: 6630-65-5
9-chlorofluorene

: 835-17-6
9-(dichloromethylene)fluorene

Guidance literature:: With ammonia; copper(l) chloride; In water; dimethyl sulfoxide; at 20 ℃;
DOI:10.1023/A:1023499925287

Reference yield:

: 197901-71-6
9-fluorenyl trichloromethyl sulfoxide

: 486-25-9,952573-42-1
9-fluorenone

: 4440-32-8
9-Thiofluorenone S-oxide

: 835-17-6
9-(dichloromethylene)fluorene

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 25 ℃; for 1h; Yield given. Yields of byproduct given;
DOI:10.1016/S0040-4020(97)00904-6

Reference yield: 40.0%

: 835-17-6
9-(dichloromethylene)fluorene

: 829-85-6
diphenylphosphane

: C₃₈H₂₈P₂

Guidance literature:: With bis(triphenylphosphine)nickel(II) chloride; triethylamine; In N,N-dimethyl-formamide; at 120 ℃; for 18h;
DOI:10.1021/acscatal.0c04199