3-Cyclohexen-1-ol, 3-(10-hydroxy-7-methyl-3,7-decadienyl)-4-methyl-, (E,E)-

Base Information

Chemical Name:3-Cyclohexen-1-ol, 3-(10-hydroxy-7-methyl-3,7-decadienyl)-4-methyl-, (E,E)-
CAS No.:92844-01-4
Molecular Formula:C₁₈H₃₀O₂
Molecular Weight:278.435
Hs Code.:

Synonyms:

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Chemical Property of 3-Cyclohexen-1-ol, 3-(10-hydroxy-7-methyl-3,7-decadienyl)-4-methyl-, (E,E)-

Chemical Property:

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Technology Process of 3-Cyclohexen-1-ol, 3-(10-hydroxy-7-methyl-3,7-decadienyl)-4-methyl-, (E,E)-

There total 25 articles about 3-Cyclohexen-1-ol, 3-(10-hydroxy-7-methyl-3,7-decadienyl)-4-methyl-, (E,E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14774-35-7
(S)-tetrahydropyran-3-yl-carboxaldehyde

: 92844-01-4
3-((3E,7E)-10-Hydroxy-7-methyl-deca-3,7-dienyl)-4-methyl-cyclohex-3-enol

Guidance literature:: Multi-step reaction with 9 steps

1: 93 percent / PBr₃ / diethyl ether / 0 °C

2: 1) Na, 2) 1.1 M KOH / 2) 18-cronw-6 / 1) EtOH, r.t., 2) EtOH, r.t. to reflux

3: 100 percent / 10percent aq. NaOH / Heating

4: 76 percent / Li, EtNH₂ / 10 h / -78 °C

5: 53 percent / imidazole / dimethylformamide / Ambient temperature

6: 66 percent / LiAlH₄ / tetrahydrofuran / Ambient temperature

7: 89 percent / Collins reagent

8: 80 percent / PhLi / tetrahydrofuran; diethyl ether / -78 - -30 °C

9: 1) nBu₄NF, 2) Li, NH₃ / 1) THF, r.t., 2) THF, -40 deg C

With 1H-imidazole; potassium hydroxide; sodium hydroxide; lithium aluminium tetrahydride; Collins oxidation agent; tetrabutyl ammonium fluoride; ammonia; sodium; phosphorus tribromide; lithium; ethylamine; phenyllithium; 2) 18-cronw-6; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1039/c39840000721

Reference yield:

: 22428-87-1
4,4-ethylenedioxycyclohexan-1-ol

: 92844-01-4
3-((3E,7E)-10-Hydroxy-7-methyl-deca-3,7-dienyl)-4-methyl-cyclohex-3-enol

Guidance literature:: Multi-step reaction with 14 steps

1: 93 percent / NaH / tetrahydrofuran / Heating

2: 75 percent / 2 M aq. H₂SO₄ / acetone / Heating

3: 98 percent / HCl / ethanol / Heating

4: 85 percent / diethyl ether / Ambient temperature

5: DBU / tetrahydrofuran / 4 h / -5 °C

6: diethyl ether / -78 °C

7: 62 percent / Hg(OAc)2 / Heating

8: Claisen rearrangement

9: 92 percent / LiAlH₄ / tetrahydrofuran

10: 85 percent / pyridine / 0 °C

11: 88 percent / NaI / acetone / Ambient temperature

12: 84 percent / benzene / 84 °C

13: 80 percent / PhLi / tetrahydrofuran; diethyl ether / -78 - -30 °C

14: 1) nBu₄NF, 2) Li, NH₃ / 1) THF, r.t., 2) THF, -40 deg C

With hydrogenchloride; lithium aluminium tetrahydride; sulfuric acid; mercury(II) diacetate; tetrabutyl ammonium fluoride; ammonia; lithium; sodium hydride; phenyllithium; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide; In tetrahydrofuran; pyridine; diethyl ether; ethanol; acetone; benzene;
DOI:10.1039/c39840000721

Reference yield:

: 459-88-1
(E)-4,8-dimethylnona-3,7-dien-1-ol

: 92844-01-4
3-((3E,7E)-10-Hydroxy-7-methyl-deca-3,7-dienyl)-4-methyl-cyclohex-3-enol

Guidance literature:: Multi-step reaction with 6 steps

1: 91 percent / imidazole / dimethylformamide / 16 h / 42 °C

2: 66 percent / NBS, H₂O / tetrahydrofuran / 3 h / 5 °C

3: 90 percent / K₂CO₃ / methanol

4: 88 percent / HIO₄ / diethyl ether / 0.5 h / Ambient temperature

5: 80 percent / PhLi / tetrahydrofuran; diethyl ether / -78 - -30 °C

6: 1) nBu₄NF, 2) Li, NH₃ / 1) THF, r.t., 2) THF, -40 deg C

With 1H-imidazole; N-Bromosuccinimide; tetrabutyl ammonium fluoride; ammonia; water; lithium; potassium carbonate; phenyllithium; periodic acid; In tetrahydrofuran; methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1039/c39840000721