alpha-D-Galactopyranosiduronic acid, methyl methyl ester, triacetate

Base Information

Chemical Name:alpha-D-Galactopyranosiduronic acid, methyl methyl ester, triacetate
CAS No.:35785-35-4
Molecular Formula:C14H20O10
Molecular Weight:348.3026
Hs Code.:

Synonyms:alpha-D-Galactopyranosiduronic acid, methyl methyl ester, triacetate;SCHEMBL12442266;35785-35-4;FT-0672256;.alpha.-D-Galactopyranosiduronic acid,methyl methyl ester,triacetate;Methyl 2,3,4-Tri-O-acetyl- beta -D-glucuronic Acid Methyl Ester

Suppliers and Price of alpha-D-Galactopyranosiduronic acid, methyl methyl ester, triacetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of alpha-D-Galactopyranosiduronic acid, methyl methyl ester, triacetate

Chemical Property:

Vapor Pressure:4.25E-06mmHg at 25°C
Boiling Point:383.9°Cat760mmHg
Flash Point:165.8°C
Density:1.29g/cm³
XLogP3:-0.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:10
Rotatable Bond Count:9
Exact Mass:348.10564683
Heavy Atom Count:24
Complexity:502

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)OC1C(C(OC(C1OC(=O)C)OC)C(=O)OC)OC(=O)C

Technology Process of alpha-D-Galactopyranosiduronic acid, methyl methyl ester, triacetate

There total 39 articles about alpha-D-Galactopyranosiduronic acid, methyl methyl ester, triacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.4%

: 67-56-1
methanol

: 21085-72-3
1-bromo-2,3,4-tri-O-acetyl-α-D-glucuronic acid methyl ester

: 30902-96-6,34213-34-8,35785-35-4,50767-72-1,63730-53-0,63730-54-1,63730-55-2,74033-69-5,77880-64-9,87936-90-1,108032-42-4,136520-47-3
methyl (methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid)uronate

Guidance literature:: With silver carbonate; In toluene; at 20 - 75 ℃; for 21h; Inert atmosphere;
DOI:10.1016/j.carres.2012.01.002

Reference yield: 64.0%

: 67-56-1
methanol

: 92420-89-8
methyl 2,3,4-tri-O-acetyl-1-O-(trichloroacetimidoyl)-α-D-glucopyranuronate

: 30902-96-6,34213-34-8,35785-35-4,50767-72-1,63730-53-0,63730-54-1,63730-55-2,74033-69-5,77880-64-9,87936-90-1,108032-42-4,136520-47-3
methyl (methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid)uronate

Guidance literature:: methanol; methyl 2,3,4-tri-O-acetyl-1-O-(trichloroacetimidoyl)-α-D-glucopyranuronate; In dichloromethane; at -10 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

With boron trifluoride diethyl etherate; In dichloromethane; at -10 ℃; Molecular sieve; Inert atmosphere;
DOI:10.1002/chem.201903788

Reference yield: 48.0%

: 107952-58-9
methyl uronate

: 108032-42-4
methyl (methyl 2,3,4-tri-O-acetyl-α-L-idopyranoside)uronate

: 30902-96-6,34213-34-8,35785-35-4,50767-72-1,63730-53-0,63730-54-1,63730-55-2,74033-69-5,77880-64-9,87936-90-1,108032-42-4,136520-47-3
methyl (methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid)uronate

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 2h; stereoselective reaction; Inert atmosphere; Reflux;
DOI:10.1039/c6ob00283h