2-Oxa-7,9-diazabicyclo[4.2.2]decane-8,10-dione, 5-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-9-(phenylmethyl)-7-[phen yl(trimethylsilyl)methyl]-

Base Information

Chemical Name:2-Oxa-7,9-diazabicyclo[4.2.2]decane-8,10-dione, 5-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-9-(phenylmethyl)-7-[phen yl(trimethylsilyl)methyl]-
CAS No.:95694-67-0
Molecular Formula:C31H46N2O4Si2
Molecular Weight:566.888
Hs Code.:

2-Oxa-7,9-diazabicyclo[4.2.2]decane-8,10-dione,
5-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-9-(phenylmethyl)-7-[phen
yl(trimethylsilyl)methyl]-

Synonyms:

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Chemical Property of 2-Oxa-7,9-diazabicyclo[4.2.2]decane-8,10-dione, 5-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-9-(phenylmethyl)-7-[phen yl(trimethylsilyl)methyl]-

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Technology Process of 2-Oxa-7,9-diazabicyclo[4.2.2]decane-8,10-dione, 5-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-9-(phenylmethyl)-7-[phen yl(trimethylsilyl)methyl]-

There total 11 articles about 2-Oxa-7,9-diazabicyclo[4.2.2]decane-8,10-dione, 5-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-9-(phenylmethyl)-7-[phen yl(trimethylsilyl)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 92098-02-7
1,4-dibenzyl-3-(2'-thiopyridyl)-6-<1''-(hydroxymethyl)-3''-(hydroxypropyl)>-2,5-piperazinedione

: 95694-67-0
8-benzyl-10-<(tert-butyldimethylsilyl)benzyl>-8,10-diaza-5-<((tert-butyldimethylsilyl)oxy)methyl>-2-oxabicyclo<4.2.2>decane-7,9-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 13.5 percent / (dimethylamino)pyridine, triethylamine / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 91 percent / silver triflate / tetrahydrofuran / 0.33 h / Ambient temperature

With dmap; silver trifluoromethanesulfonate; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00297a035

Reference yield:

: 92098-01-6
1,4-dimethyl-3-(2'-thiopyridyl)-6-(2''-δ-valerolactonyl)-2,5-piperazinedione (syn, major diastereomer)

: 95694-67-0
8-benzyl-10-<(tert-butyldimethylsilyl)benzyl>-8,10-diaza-5-<((tert-butyldimethylsilyl)oxy)methyl>-2-oxabicyclo<4.2.2>decane-7,9-dione

Guidance literature:: Multi-step reaction with 4 steps

1: 54 percent / lithium aluminium hydride / tetrahydrofuran / 0.5 h / 0 °C

2: 13.5 percent / (dimethylamino)pyridine, triethylamine / CH₂Cl₂ / 0.5 h / Ambient temperature

3: 91 percent / silver triflate / tetrahydrofuran / 0.33 h / Ambient temperature

With dmap; lithium aluminium tetrahydride; silver trifluoromethanesulfonate; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00297a035

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 95694-67-0
8-benzyl-10-<(tert-butyldimethylsilyl)benzyl>-8,10-diaza-5-<((tert-butyldimethylsilyl)oxy)methyl>-2-oxabicyclo<4.2.2>decane-7,9-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 13.5 percent / (dimethylamino)pyridine, triethylamine / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 91 percent / silver triflate / tetrahydrofuran / 0.33 h / Ambient temperature

With dmap; silver trifluoromethanesulfonate; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00297a035