Gallium, bis(ethanethiolato)phenyl-

Base Information

• Chemical Name: Gallium, bis(ethanethiolato)phenyl-
• CAS No.: 95926-61-7
• Molecular Formula: C₁₀H₁₅GaS₂
• Molecular Weight: 269.084
• Mol file: 95926-61-7.mol

Synonyms:

Chemical Property of Gallium, bis(ethanethiolato)phenyl-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Gallium, bis(ethanethiolato)phenyl-

There total 1 articles about Gallium, bis(ethanethiolato)phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.3%

triphenylgallane (1088-02-4) + ethanethiol (75-08-1) → phenyl(diethylthio)gallane (95926-61-7)

Guidance literature:

In benzene; byproducts: benzene; a benzene soln. of thiol (2 equiv) was added dropwise under N2 to a benzene soln. of Ph3Ga, mixt. was stirred for 30 min at room temp.; soln. was decanted from the ppt., evapd.; elem. anal.;

DOI:10.1016/0022-328X(84)80699-3

Reference yield: 87.0%

phenyl(diethylthio)gallane (95926-61-7) + trimethylamine (75-50-3) → phenyl(diethylthio)gallane-trimethylamine

Guidance literature:

In dichloromethane; dry Me3N was bubbled through a soln. of gallane in CH2Cl2 for 15 min, mixt. was stirred for addnl. 30 min; soln. was decanted, decantate evapd.; elem. anal.;

DOI:10.1016/0022-328X(84)80699-3

upstream raw materials:

triphenylgallane

ethanethiol