Pyridine, 2-chloro-6-(1,1-dimethylethyl)-

Base Information

• Chemical Name: Pyridine, 2-chloro-6-(1,1-dimethylethyl)-
• CAS No.: 97691-23-1
• Molecular Formula: C9H12ClN
• Molecular Weight: 169.654

Synonyms:2-tert-butyl-6-chloropyridine;2-tert-Butyl-6-chloro-pyridine;2-chloro-6-t-butylpyridine;6-tertbutyl-2-chloropyridine;

Chemical Property of Pyridine, 2-chloro-6-(1,1-dimethylethyl)-

Chemical Property:

• Boiling Point: 81 - 82 °C (15 mmHg)
• PSA: 12.89000
• LogP: 3.03250

Purity/Quality:

99% ^*data from raw suppliers

2-chloro-6-(1,1-dimethylethyl)-Pyridine 97.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Pyridine, 2-chloro-6-(1,1-dimethylethyl)-

There total 9 articles about Pyridine, 2-chloro-6-(1,1-dimethylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2,6-dichloropyridine (2402-78-0) + tert-butylmagnesium chloride (677-22-5) → 2-(tert-butyl)-6-chloropyridine (97691-23-1)

Guidance literature:

With copper(l) iodide; In tetrahydrofuran; at 0 - 20 ℃; for 6h;

DOI:10.1002/anie.200803312

Reference yield: 71.0%

6-tert-butylpyridin-2(1H)-one (58498-57-0) → 2-(tert-butyl)-6-chloropyridine (97691-23-1)

Guidance literature:

6-tert-butylpyridin-2(1H)-one; With trichlorophosphate; In N,N-dimethyl-formamide; at 120 ℃; for 2h; Inert atmosphere;

With phosphorus pentachloride; for 1h; Reflux; Inert atmosphere;

DOI:10.1002/chem.200900563

Reference yield: 48.0%

6-tert-butyl-2-hydroxypyridine (58498-57-0) → 2-(tert-butyl)-6-chloropyridine (97691-23-1)

Guidance literature:

With phosphorus pentachloride; trichlorophosphate; at 160 ℃; for 1h;

DOI:10.1002/1099-0682(200007)2000:7<1411::AID-EJIC1411>3.0.CO;2-M

upstream raw materials:

2-chloropyridine

tert-butylmercury chloride

6-chloro-2-picoline

6-tert-butyl-2-hydroxypyridine

Downstream raw materials:

2-tert-butyl-6-diphenylphosphinopyridine

6,6'-di-tert-butyl-2,2'-bipyridine

6-(tert-butyl)-2-chloronicotinaldehyde

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